Search results for "grain"

The effects of cryogenic cooling on surface integrity in hard machining: A comparison with dry machining

2012

Abstract This paper presents results of an experimental study of cryogenic machining of hardened AISI 52100 steel, focusing on surface integrity. Experiments were performed under dry and cryogenic cooling conditions using CBN tools varying cutting speeds, workpiece hardness and tool geometry. Surface integrity parameters (surface roughness, white layer thickness, residual stresses, metallurgical conditions including grain size, phase transformation, etc.) were investigated to establish the effects of cryogenic cooling on the surface integrity of the machined component, and results were compared with those from dry hard machining. Overall, cryogenic cooling provides improved surface integrit…

Peculiarities of Forming of Magnetic Hardening in Sintered Nd15Fe76.2Ti1.0Al0.8B7 Permanent Magnet by Ageing

1999

Variations of the intrinsic coercivity ( i H c ) with ageing (at 293 to 1173 K for 0.45 to 57.6 ks) of sintered Nd 15 Fe 76.2 Ti 1.0 Al 0.8 B 7 have been investigated. The tests indicated minimum and maximum of intrinsic coercivity ( i H min c and i H max c ) at temperatures 725 K and 1025 K, respectively. The observed behaviour of i H c has been compared with microhardness measurements and microstructure observations (SEM, EDAX, domain structure (DS) and room temperature Mossbauer spectroscopy). SEM and DS investigations gave hints to a change in microstructure. Fitting of the Mossbauer spectra of permanent magnets for different i H c has shown that the magnetic hyperfine field Bhf of 8j2 …

Effect of zinc concentration on the microstructure and relaxation frequency of Mn–Zn ferrites synthesized by solid state reaction

2013

Abstract Mn3Zn polycrystalline ferrites with Mn1−xZnxFe2O4 stoichiometry (x=0.59, 0.61, 0.65) were prepared by solid state reaction. These ferrites were heated at different temperatures. The cubic structure with space group Fd3m (Oh7) No. 227 was confirmed by the refinement of x-ray diffraction (XRD) powders through Rietveld´s method using fullprof. Scanning electron microscopy (SEM) results revealed for all compounds a non-homogeneous grain size and shape distribution, with a mean grain size of 9 μm. The Curie temperature Tc was found to decrease as the Zn concentration increases. The magnetic domain relaxation was investigated by inductance spectroscopy (IS). The relaxation frequency fr s…

Hexagonal boron nitride luminescence dependent on vacuum level and surrounding gases

2015

Abstract Gas sensing properties of hBN powder bulk and nanosize were studied. It was demonstrated that for hBN powders with grain sizes of 70 nm, 1 μm and 5 μm the native defect-induced luminescence observed at 400 nm under 265 nm light excitation and room temperature is sensitive to oxygen gas reducing luminescence intensity. The highest value of luminescence intensity is reached when sample is in vacuum. Results obtained allow conclusion that the hBN powder is prospective for sensing of oxygen gas. Some material properties such as dependence of luminescence intensity on vacuum level and pumping time, ratio of luminescence intensity when sample is in vacuum and gas, its dependence on mater…

Behaviour of tritium in breeding materials

2005

Abstract The tritium release from ceramic materials of the HCPB under real DEMO operating conditions will depend not only on temperature and neutron flux but also on an intense magnetic field (MF) of 7–9 T. The delay in the tritium release induced by the MF is proportional to the grain size of the ceramics, the squared MF intensity and the abundance ratio of charged tritium forms (T + , T − ) in the grain volume of the ceramics. The effect of MFs of different intensity on the tritium release from the Li 4 SiO 4 pebbles irradiated in the EXOTIC-8 experiment (neutron fluence 2.4 × 10 25  n m −2 , irradiation temperature up to 700 K) was investigated in this study. As a result of the irradiati…

Mechanical and microstructural characterization of friction stir welded skin and stringer joints

2013

A microstructural and mechanical investigation on lap joints welded by friction stir welding and made out of a 7075-T6 stringer and a 2024-T4 skin is presented. In particular, the metallurgical and mechanical properties of joints have been studied at different tool feed rates (V = 35, 50, 100 mm/min) and constant rotation speed (R = 500 r/min). Temperature distributions have been monitored during the process. It is found that in the welded area, the recrystallized zone (nugget) has an average grain size of about 3 µm and exhibits coarsened MgZn2 particles on grain boundaries. The maximum values of microhardness in the welded skin increase with the process temperature, while they just sligh…

Texture Effects on Zircaloy Oxidation : Experiment and Simulation

2002

CDRX modelling in friction stir welding of aluminium alloys

2005

In the paper a numerical model aimed to the determination of the average grain size due to continuous dynamic recrystallization phenomena (CDRX) in friction stir welding processes of AA6082 T6 aluminum alloys is presented. In particular, the utilized model takes into account the local effects of strain, strain rate and temperature; an inverse identification approach, based on a linear regression procedure, is utilized in order to develop the proper material characterization.

Influence of sintering temperature on microstructure of Na0.5Bi0.5TiO3 ceramics

2021

Abstract Na0.5Bi0.5TiO3 (NBT)-based compositions are among the most promising lead-free ferroelectrics. Although studies of modification of NBT-based compositions’ properties are a hot topic, there has been very little attention paid to their characterization from the standpoint of ceramics and the process of producing them. Here, we report on comprehensive analysis of the influence of sintering temperature across a wide temperature range (1020–1240 °C) on the complete microstructure and chemical content of NBT ceramics produced by solid state sintering, which is dominating in producing of NBT ceramics. Thorough attention is paid to the grain size distribution, porosity, and inhomogeneity. …

A microstructural model for homogenisation and cracking of piezoelectric polycrystals

2019

Abstract An original three-dimensional generalised micro-electro-mechanical model for computational homogenisation and analysis of degradation and micro-cracking of piezoelectric polycrystalline materials is proposed in this study. The model is developed starting from a generalised electro-mechanical boundary integral representation of the micro-structural problem for the individual bulk grains and a generalised cohesive formulation is employed for studying intergranular micro-damage initiation and evolution into intergranular micro-cracks. To capture the electro-mechanical coupling at the evolving damaging intergranular interfaces, standard mechanical cohesive laws are enriched with suitab…