Search results for "microwave"
showing 10 items of 693 documents
Microwave-assisted synthesis of anhydrous CdS nanoparticles in a water-oil microemulsion.
2006
Abstract Microwave irradiation at a frequency of 2.45 GHz and a power ranging between 22 and 30 W was used, in a water–oil microemulsion at 35 ± 2 ° C , to obtain stable, small, crystalline, anhydrous CdS nanoparticles exhibiting enhanced luminescence properties. The process of nanoparticles growth at different irradiation times was followed by UV–vis spectroscopy. It was observed that irradiated nanoparticles grew faster and their size reached a constant value. The final mean nanoparticle diameter was 2.7 nm, smaller than that observed in a non-irradiated sample, in which particle dimensions slowly increased even after 10 h. This finding was confirmed by high resolution transmission electr…
Level anti-crossing magnetometry with color centers in diamond
2017
Recent developments in magnetic field sensing with negatively charged nitrogen-vacancy centers (NV) in diamond employ magnetic-field (MF) dependent features in the photoluminescence (PL) and eliminate the need for microwaves (MW). Here, we study two approaches towards improving the magnetometric sensitivity using the ground-state level anti-crossing (GSLAC) feature of the NV center at a background MF of 102.4\,mT. Following the first approach, we investigate the feature parameters for precise alignment in a dilute diamond sample; the second approach extends the sensing protocol into absorption via detection of the GSLAC in the diamond transmission of a 1042\,nm laser beam. This leads to an …
Morphological and optical property study of Li doped ZnO produced by microwave-assisted solvothermal synthesis
2021
Abstract ZnO materials have been at the centre of many studies for decades. Doping of ZnO by lithium atoms is a prospective approach for compensation of n-type conductivity in the unintentionally doped ZnO aimed at obtaining p-type semiconductor. In this study, we have synthesized ZnO rod-like powders doped with lithium ions (0–0.65 atom%) by the new microwave-assisted solvothermal method in order to obtain greater photoluminescence intensity of ZnO emissions in the UV region. The obtained powders contain nanoparticles from 20 nm up to 250 nm depending on Li content. X-ray diffractometry and Raman spectroscopy were employed to characterise the structure of ZnO powders, scanning electron mic…
Microwave radiation effect on the synthesis of cadmium sulphide nanoparticles in water in oil microemulsion: a preliminary study at different frequen…
2004
AbstractCadmium sulphide nanoparticles have been synthesised in water/sodium bis (2-ethylhexyl) sulfosuccinate (AOT)/n- heptane microemulsions kept at 30 °C by microwave irradiation coupled with water-cooling and in conventional thermostatic conditions at the same temperature. The study has been performed exposing the reaction media to microwave radiation at five different frequencies (2.45, 2.85, 8, 12 and 18 GHz). For each frequency, a suitable microwave exposure set-up has been assembled. During the growth process, the dimensions of the nanoparticles have been characterised by means of UV-Vis spectroscopy. At the end of the growth process, the surface morphology of the nanoparticles has …
Hypersensitive tunable Josephson escape sensor for gigahertz astronomy
2020
Sensitive photon detection in the gigahertz band constitutes the cornerstone to study different phenomena in astronomy, such as radio burst sources, galaxy formation, cosmic microwave background, axions, comets, gigahertz-peaked spectrum radio sources and supermassive black holes. Nowadays, state of the art detectors for astrophysics are mainly based on transition edge sensors and kinetic inductance detectors. Overall, most sensible nanobolometers so far are superconducting detectors showing a noise equivalent power (NEP) as low as 2x10-20 W/Hz1/2. Yet, fast thermometry at the nanoscale was demonstrated as well with Josephson junctions through switching current measurements. In general, det…
The 3 Cavity Prototypes of RADES: An Axion Detector Using Microwave Filters at CAST
2019
The Relic Axion Detector Experimental Setup (RADES) is an axion search project that uses a microwave filter as resonator for Dark Matter conversion. The main focus of this publication is the description of the 3 different cavity prototypes of RADES. The result of the first tests of one of the prototypes is also presented. The filters consist of 5 or 6 stainless steel sub-cavities joined by rectangular irises. The size of the sub-cavities determines the working frequency, the amount of sub-cavities determine the working volume. The first cavity prototype was built in 2017 to work at a frequency of $\sim$ 8.4 GHz and it was placed at the 9 T CAST dipole magnet at CERN. Two more prototypes wer…
Gas-Phase Spectroscopic Detection and Structural Elucidation of Carbon-Rich Group 14 Binary Clusters: Linear GeC3Ge
2016
Guided by high-level quantum-chemical calculations at the CCSD(T) level of theory, the first polyatomic germanium-carbon cluster, linear Ge2C3, has been observed at high spectral resolution in the gas phase through its remarkably complex fundamental antisymmetric C-C stretching mode ν3 located at 1932 cm(-1). The observation of a total of six isotopic species permits the derivation of a highly accurate value for the equilibrium Ge-C bond length. The present study suggests that many more Ge-C species might be detectable in the future using a combination of laser-ablation techniques for production and high-resolution infrared and/or microwave techniques for spectroscopic detection.
New Neutrino Mass Bounds from SDSS-III Data Release 8 Photometric Luminous Galaxies
2012
We present neutrino mass bounds using 900,000 luminous galaxies with photometric redshifts measured from Sloan Digital Sky Survey III Data Release 8. The galaxies have photometric redshifts between z = 0.45 and z = 0.65 and cover 10,000 deg(2), thus probing a volume of 3 h(-3) Gpc(3) and enabling tight constraints to be derived on the amount of dark matter in the form of massive neutrinos. A new bound on the sum of neutrino masses Sigma m nu < 0.27 eV, at the 95% confidence level (CL), is obtained after combining our sample of galaxies, which we call CMASS with Wilkinson Microwave Anisotropy Probe (WMAP) seven-year cosmic microwave background data and the most recent measurement of the Hubb…
ESTIMATING SMALL ANGULAR SCALE COSMIC MICROWAVE BACKGROUND ANISOTROPY WITH HIGH-RESOLUTIONN-BODY SIMULATIONS: WEAK LENSING
2010
We estimate the impact of weak lensing by strongly nonlinear cosmological structures on the cosmic microwave background. Accurate calculation of large l multipoles requires N-body simulations and ray-tracing schemes with both high spatial and temporal resolution. To this end, we have developed a new code that combines a gravitational Adaptive Particle-Particle, Particle-Mesh solver with a weak-lensing evaluation routine. The lensing deviations are evaluated while structure evolves during the simulation so that all evolution steps—rather than just a few outputs—are used in the lensing computations. The new code also includes a ray-tracing procedure that avoids periodicity effects in a univer…
Magnetic skyrmions: from fundamental to applications
2016
In this topical review, we will discuss recent advances in the field of skyrmionics (fundamental and applied aspects) mainly focusing on skyrmions that can be realized in thin film structures where an ultrathin ferromagnetic layer (<1 nm) is coupled to materials with large spin-orbit coupling. We review the basic topological nature of the skyrmion spin structure that can entail a stabilization due to the chiral exchange interaction present in many multilayer systems with structural inversion asymmetry. The static spin structures and the dynamics of the skyrmions are also discussed. In particular, we show that skyrmions can be displaced with high reliability and efficiency as needed for t…