Search results for "rafting"

Il Drafting

2012

La qualità della redazione dei testi normativi, tanto nel contenuto, quanto nella struttura, costituisce un'esigenza che connota anche la produzione normativa delle regioni. In particolare presso l'Assemblea della regione Sicilia opera dal 2008 un apposito Comitato per la qualità della legislazione che, insieme al servizio delle Commissioni, rappresenta un supporto insostituibile per le Commissioni consiliari e per la stessa Aula. Esso interviene nel corso del procedimento di formazione delle leggi e dei testi unici, formulando un parere relativo alla omogeneità, chiarezza, proprietà di formulazione, nonchè all'efficacia dei testi ai fini del riordino e della semplificazione della legislazi…

Bentonites with grafted aminogroups: Synthesis, protolytic properties and assessing Cu(II), Cd(II) and Pb(II) adsorption capacity

2019

Abstract Bentonites with grafted methylaminopropyl (NHCH3-Bent), aminopropyl (NH2-Bent), ethylenediaminopropyl (En-Bent) and diethylenetriaminopropyl (Dien-Bent) groups were synthesized by silylation procedure. The successful covalent grafting of silylating agents on the bentonite was confirmed by 29Si NMR, FTIR and thermal analysis. The effects of polar (ethanol) and non-polar (dioxane) solvents on grafting process were compared. The samples prepared in ethanol showed the increase of d001 value from initial 1.44 nm to 1.63–2.05 nm proportionally to the loading amount of grafted silane. However, an almost constant value of d001 (1.96–2.10 nm) was observed for all samples obtained in dioxane…

Evaluation of Risk Parameters in Bone Regeneration Using a Customized Titanium Mesh

2019

PURPOSE The aim of the study was an evaluation of risk factors for an innovative bone regeneration technique using a customized titanium mesh that was tested in a clinical setting. MATERIALS AND METHODS This retrospective study included 65 patients with 70 grafting procedures of osseous defects of the jaws with a customized titanium mesh together with Advanced- and Injectable-Platelet-Rich Fibrin (A- and I-PRF), resorbable membranes, and bone grafting materials. Exposures of the meshes and grafting outcome were analyzed according to a novel classification as (a) punctual and (b) tooth width or complete exposure of the mesh (c). No exposure was stated as (d). RESULTS In 37% of cases, exposur…

The influence of bone allograft processing on osteoblast attachment and function

2004

In order to assess the influence of eight different sterilisation and disinfection methods for bone allografts on adhesion, proliferation, and differentiation of human bone marrow stromal cells (BMSC), cells were grown in culture and then plated onto pieces of human bone allografts. Following processing methods were tested: autoclavation (AUT), low-temperature-plasma sterilisation of demineralised allografts (D-LTP), ethylene oxide sterilisation (EtO), fresh frozen bone (FFB), 80 degrees C-thermodisinfection (80 degrees C), gamma-irradiation (Gamma), chemical solvent disinfection (CSD), and Barrycidal-disinfection (BAR). The seeding efficiency was determined after one hour to detect the num…

Dispersion Copolymerization of Vinyl Monomers in Supercritical Carbon Dioxide.

2003

The thermally initiated free-radical dispersion copolymerization of methyl methacrylate (MMA) and N,N-dimethylacrylamide (DMA) in supercritical carbon dioxide has been studied in the presence of polysiloxane surfactants. The formation of a stable latex seems to be related to the presence of at least one reactive end group in the surfactant macromolecule, thus suggesting that anchoring of the stabilizer to the surface of the growing polymer particles occurs through chemical grafting. In the case of a molar ratio of DMA to MMA lower than 0.40, microspherical copolymer particles with yields ranging from 81 to 97% were collected from batch polymerizations carried out at 65 °C and 23-28 MPa usin…

Grafting of (3-chloropropyl)-trimethoxy silane on halloysite nanotubes surface

2021

Modified halloysite nanotubes (HNTs-Cl) were synthesized by a coupling reaction with (3-chloropropyl) trimethoxysilane (CPTMS). The incorporation of chloro-silane onto HNTs surface creates HNTs-Cl, which has great chemical activity and is considered a good candidate as an active site that reacts with other active molecules in order to create new materials with great applications in chemical engineering and nanotechnology. The value of this work lies in the fact that improving the degree of grafting of chloro-silane onto the HNT’s surface has been accomplished by incorporation of HNTs with CPTMS under different experimental conditions. Many parameters, such as the dispersing media, the molar…

Autogenous teeth used for bone grafting: A systematic review

2018

Background Recently, bone graft materials using permanent teeth have come to light, and clinical and histological outcomes of this material have been confirmed by some studies. The aim of this systematic review was to evaluate the reliability of the autogenous tooth bone graft material applied to alveolar ridge augmentation procedures. Material and Methods A systematic review of literature was conducted analyzing articles published between 2007 and 2017. The following four outcome variables were defined: a) implant stability b) post-operative complication c) evaluation of implant survival and failure rates, and d) histological analysis. A total of 108 articles were identified; 6 were select…

Magnetic Resonance Imaging and Ultrasound Evaluation after Breast Autologous Fat Grafting Combined with Platelet-Rich Plasma

2014

Health-Improved Textiles Obtained by Heat Surface Ecodyeing Treatments

2015

The central idea of the present research aims at achieving textile substrates through an efficient inclusion of a wild black cherry extract into the grafting agent-monochlorotriazinyl-β-cyclodextrin (MCT-β-CD). The methodology consists in a permanent/irreversible entrapment onto the fibres surface of the natural extract through inclusion mechanism. Exhaustion and sonication dyeing procedures were used alternatively. The obtained materials were characterized, by FT-IR and BET analysis. The experimental results reveal good adsorptive feature of the samples, due to a higher specific surface created by the inclusion complex (MCT-β-CD-dye pigment). An efficient blocking of the natural dye pigmen…

One step grafting of monomethoxy poly(ethylenglycol) during synthesis of maghemite nanoparticles in aqueous medium

2008

Abstract Grafting of silanated monomethoxy poly(ethylene glycol) (m-PEG) onto maghemite nanoparticles surface in aqueous medium through one step procedure was investigated. The major characteristic of this work is that the grafting of m-PEG was produced during the synthesis of maghemite nanoparticles. The maghemite nanoparticles were characterized by photon correlation spectroscopy (PCS), zeta potential measurement, X-ray diffraction (XRD), Raman spectroscopy, transmission electron microscopy (TEM), Fourier transform infrared spectrometer (FTIR), and X-ray photoelectron spectroscopy (XPS). The spinel structure of maghemite nanoparticles was verified and successful grafting of m-PEG was evid…