Search results for "recrystallization"
showing 10 items of 76 documents
P-T path development derived from shearband boudin microstructure
2016
This work focuses on the development of a regional P-T-path from the Malpica-Lamego Ductile Shear Zone, NW Portugal, based on the microstructures of shearband boudins evolved during progressive simple shear. The combination of microstructural analysis, fluid inclusion studies, crystallographic pre- ffered orientation and fractal geometry analyses, allows to link several stages in the internal evolution of the boudin to regional P-T conditions. The boudinage process is initiated under differential stress after the original layer achieved sufficient viscosity contrast relative to the surrounding matrix. Two main transformations occur simultaneously: i) change in the external shape with contin…
High-Fluence Implantation of Erbium into Silicon-Germanium Alloys: Structural and Thermal Properties
2000
AbstractHigh-quality crystalline Si1-xGex (x=0.10 and 0.25) alloys were implanted with 70 keV Er+ ions at temperatures of 350°C and 550°C to a fluence of 1015 cm−2. In-situ Rutherford backscattering/channeling (RBS) analysis supplemented with transmission electron microscopy (TEM) showed that as-implanted alloys were in form of ternary solid solutions with a peak Er concentration of 1 at.% without any trace of Er-Si or Er-Ge precipitation.In the samples implanted at 350°C Er atoms were found to be distributed randomly in the amorphous host matrix. Post-implantation annealing at different temperatures up to 600° showed that the solid phase epitaxial regrowth of the damaged layers strongly de…
The influence of strain rate and presence of dispersed second phases on the deformation behaviour of polycrystalline D2O ice
2018
ABSTRACTThis contribution discusses results obtained from 3-D neutron diffraction and 2-D fabric analyser in situ deformation experiments on laboratory-prepared polycrystalline deuterated ice and ice containing a second phase. The two-phase samples used in the experiments are composed of an ice matrix with (1) air bubbles, (2) rigid, rhombohedral-shaped calcite and (3) rheologically soft, platy graphite. Samples were tested at 10°C below the melting point of deuterated ice at ambient pressures, and two strain rates of 1 × 10−5 s−1 (fast) and 2.5 × 10−6 s−1 (medium). Nature and distribution of the second phase controlled the rheological behaviour of the ice by pinning grain boundary migratio…
Microstructure and fabric development in ice: Lessons learned from in situ experiments and implications for understanding rock evolution
2014
Abstract In this contribution we present a review of the evolution of microstructures and fabric in ice. Based on the review we show the potential use of ice as an analogue for rocks by considering selected examples that can be related to quartz-rich rocks. Advances in our understanding of the plasticity of ice have come from experimental investigations that clearly show that plastic deformation of polycrystalline ice is initially produced by basal slip. Interaction of dislocations play an essential role for dynamic recrystallization processes involving grain nucleation and grain-boundary migration during the steady-state flow of ice. To support this review we describe deformation in polycr…
New binary solid dispersion of indomethacin with surfactant polymer: From physical characterization to in vitro dissolution enhancement
2009
This article investigated preparation of solid dispersions containing a poor water-soluble drug, indomethacin (IND), and a new surfactant polymer, polyoxyethylene 32 distearate (POED). Solid dispersions were prepared by the melting method and characterized by DSC, hot-stage microscopy (HSM), X-ray diffraction (XRD) and scanning electron microscopy (SEM). DSC and HSM analyses performed on IND/POED physical mixtures indicated that IND could dissolve in liquid POED. The materials showed complete miscibility at liquid state. Combination of DSC, XRD, and SEM revealed that these materials had limited miscibility at the solid state. Up to 20% w/w IND in POED, we did not detect significant modifica…
CDRX modelling in friction stir welding of AA7075-T6 aluminum alloy: analytical approaches
2007
Abstract Friction stir welding (FSW) is an energy efficient and environmentally “friendly” (no fumes, noise, or sparks) welding process, during which the workpiece are welded together in a solid-state joining process at a temperature below the melting point of the workpiece material under a combination of extruding and forging. Significant microstructural evolution takes place during FSW: in particular continuous dynamic recrystallization (CDRX) phenomena result in a highly refined grain structure in the weld nugget and strongly affect the final joint resistance. In the paper two different analytical models aimed to the determination of the average grain size due to continuous dynamic recry…
Towards Tool Path Numerical Simulation in Modified Friction Stir Spot Welding Processes
2009
Spot welding can be considered a very common joining technique in automotive and transportation industries as it permits to obtain effective lap-joints with short process times and what is more it is easily developed through robots and automated systems. Recently the Friction Stir Spot Welding (FSSW) process has been proposed as a natural evolution of the already known Friction Stir Welding (FSW) process, allowing to obtain sound spot joints that do not suffer from the insurgence of typical welding defects due to the fusion of the base material. In the paper, a modified Friction Stir Spot Welding (FSSW) process, with a spiral circular movement given to the tool after the sinking stage, is p…
Metallurgical Phenomena Modelling in Friction Stir Welding of Aluminium Alloys: Analytical vs. Neural Network Based Approaches
2008
In this paper, the metallurgical phenomena occurring in friction stir welding processes of AA6082-T6 and AA7075-T6 aluminum alloys are investigated. In particular, to predict the local values of the average grain size, either a simple analytical expression depending on a few material constants or a properly trained neural network is linked to the finite element model of the process. The utilized tools, which take as inputs the local values of strain, strain rate, and temperature, were developed starting from experimental data and numerical results.
Geochronological evidence for Archaean and Palaeoproterozoic polymetamorphism in the Central Zone of the Limpopo Belt, South Africa
2018
Abstract The Central Zone of Limpopo Belt is a polymetamorphic and complexly deformed Precambrian terrane whose tectonic evolution is still uncertain because details on the timing of its evolution are not well established. We report zircon ages for newly discovered rocks in the Central Zone which document three distinct high-grade tectono-metamorphic events at 3.22, 2.62 and 2.02 Ga. The youngest of these has been well established, but the older two events were so far largely based only on rare zircon overgrowth rims. Most of our samples were collected from a large enclave in the 2.61 Ga Bulai pluton and constitute a strongly deformed, brecciated high-grade assemblage of supracrustal rocks,…
Multiple zircon growth within early Archaean tonalitic gneiss from the Ancient Gneiss Complex, Swaziland
1988
Abstract U Pb age determinations by ion microprobe reveal multiple episodes of zircon growth and recrystallization within a single sample of tonalitic gneiss from the Ancient Gneiss Complex. The oldest episode at3644 ± 4Ma(2σ) produced the dominant type of zircon, characteristically purplish-brown and massive in texture; this probably constitutes unaltered zircon precipitated from the original magma. Recrystallization accompanied (and obscured) by early Pb loss took place within the oldest grains at3504 ± 6Ma and3433 ± 8Ma. Whole new grains grew at these times also. We interpret the post-3644 Ma growth as due to episodic deformational and metamorphic events that transformed the tonalite plu…