Search results for "small-angle"

Myoglobin embedded in saccharide amorphous matrices: water-dependent domains evidenced by small angle X-ray scattering

2010

We report Small Angle X-ray Scattering (SAXS) measurements performed on samples of carboxy-myoglobin (MbCO) embedded in low-water trehalose glasses. Results showed that, in such samples, "low-protein" trehalose-water domains are present, surrounded by a protein-trehalose-water background; such finding is supported by Infrared Spectroscopy (FTIR) measurements. These domains, which do not appear in the absence of the protein and in analogous sucrose systems, preferentially incorporate the incoming water at the onset of rehydration, and disappear following large hydration. This observation suggests that, in organisms under anhydrobiosis, analogous domains could play a buffering role against th…

MAGPACK1A package to calculate the energy levels, bulk magnetic properties, and inelastic neutron scattering spectra of high nuclearity spin clusters

2001

Relaxation of the field-induced structural anisotropy in a rotating magnetic fluid

2009

The relaxation of field-induced anisotropy in a magnetic fluid with dominant repulsion is theoretically modeled and experimentally measured by small angle neutron scattering on a sample rotating at angular velocity ω. The scattered pattern distortion scales as the Mason number Mn=ω·τq, τq being the q-dependent diffusion time of nanoparticles. The model accounts for the magnetophoretical drift in the non-homogeneous self-magnetic field of the assembly, continuously created by the thermal noise. The Mn-dependence of the pattern distortion is well described without any adjustable parameter.

Some comments on fluctuating-elasticity and local oscillator models for anomalous vibrational excitations in glasses

2011

Abstract An overview is given on the present status of the theoretical description of vibrational spectra of glasses, as seen by inelastic neutron, X-ray and light (Raman) scattering. Using the language of Green's/response functions the merits and shortcomings of a local oscillator and a generalized elasticity-theory point of view are discussed. It is pointed out that in both cases the interaction of phonons with disorder-induced irregularities leads to Rayleigh scattering (mean free path l ∝ ω − 4 ) at low enough frequencies and temperatures. In disordered solids at ambient temperature the Rayleigh scattering is usually masqued by Akhiezer-like anharmonic scattering l ∝ ω − 2 , but it can …

On the Line Shape of Backward Emitted Parametric X-Radiation

2002

Parametric X radiation, emitted in opposite direction of an electron which traverses a semi infinite single crystal on a hypothetical straight trajectory, features a Lorentzian line shape with extremely narrow width. However, small angle scattering of the electron in the Coulomb potential of the crystal atoms results in a stochastic change of the electron direction. The latter leads to a line broadening which can be understood essentially as a stochastic frequency modulation of the exponentially damped wave train. The line shape has been calculated analytically by well known probabilistic methods. Results are quoted for various reflections of a silicon single crystal at an electron beam ene…

Elastic electron scattering from the multipole moment distributions ofMg25

1977

4He+Ni elastic scattering near the Coulomb barrier and optical model parameters

2002

Cross sections for the elastic scattering system of 4He+Ni have been investigated. Natural nickel was bombarded by 4He ions in the laboratory energy range of 3.0–14.3 MeV and the intensity of helium backscattering through laboratory angles of 96°, 117°, and 137° was observed. From measured yield data, the cross sections were extracted for the direct Ni(4He,4He)Ni scattering process as well as for the inverse recoil scattering process 4He(58Ni,4He)58Ni by calculating the kinematical reversal of the reaction. The experimental helium scattering angles convert to helium recoil angles of 20°, 30°, and 40°, and the incident helium ion energies to 43.5–207 MeV for incident 58Ni ions in the reverse…

SANS polarization analysis at V4 SANS instrument of HMI Berlin

2008

The V4 instrument has recently been upgraded with a 3He spin filter cell, placed directly in the homogeneous field B of the sample magnet, to enhance the SANSPOL option for polarization analysis. The prototype setup was still affected by: (a) a quick relaxation of the 3He nuclear polarization in the cell with a time constant of only ?130 min which significantly changes the spin filter transmissions T+ and T? for neutrons polarized parallel I+ and anti-parallel I? to B, and (b) the absence of a flipping aid behind the sample. The usual polarization analysis procedure, expecting virtually time-independent transmissions and a second flipping device, is therefore not applicable. We present an a…

Modeling techniques for analysing conformational transitions in hemocyanins by small-angle scattering of X-rays and neutrons.

2004

Neutron polarizability and the n-e scattering length

1972

Abstract It is shown that the neutron polarizability contribution to the n-e scattering length is within the present level of precision. The experimental result on this interaction is consistent with a value of the neutron polarizability similar to the proton one.