Search results for "traction"
showing 10 items of 3716 documents
A fast extraction procedure of 2-dodecylcyclobutanone for the identification of irradiated pork, employing gas chromatographic/mass spectrometric ana…
2008
Determination of 60 Migrant Substances in Plastic Food Contact Materials by Vortex-Assisted Liquid-Liquid Extraction and GC-Q-Orbitrap HRMS
2021
A GC-HRMS analytical method for the determination of 60 migrant substances, including aldehydes, ketones, phthalates and other plasticizers, phenol derivatives, acrylates, and methacrylates, in plastic food contact materials (FCM) has been developed and validated. The proposed method includes migration tests, according to Commission Regulation (EU) 10/2011, using four food simulants (A, B, C, and D1), followed by vortex-assisted liquid–liquid extraction (VA-LLE) and GC-Q-Orbitrap HRMS analysis in selected ion monitoring (SIM) mode, with a resolving power of 30,000 FWHM and a mass accuracy ≤5 ppm. The method was validated, showing satisfactory linearity (R2 ≥ 0.98 from 40 to 400 …
Binocular vision alterations after refractive and cataract surgery: a review.
2018
To review binocular and accommodative disorders documented after corneal or intraocular refractive surgery, in normal healthy prepresbyopic patients. A bibliographic revision was performed; it included works published before 1st July 2017 where accommodation and/or binocularity was assessed following any type of refractive surgical procedure. The search in Pubmed yielded 1273 papers, 95 of which fulfilled the inclusion criteria. Few publications reporting binocular vision and/or accommodative changes after refractive surgery in normal subjects were found. The reduction in fusional vergence is the most frequently reported alteration. Anisometropia is an important risk factor for postoperativ…
Examples of anthropogenic sinkholes in Sicily and comparison with similar phenomena in southern Italy
2013
A sinkhole, occurred in June 2011 and related to an underground quarry in the eastern sector of Marsala, is described in this paper as a case study (Figure 2). The site was selected for the availability of topographic data of the underground quarry, prior to the formation of the Abstract Anthropogenic sinkholes affect several built-up areas of Sicily (southern Italy) representing a great risk to people, buildings, and infrastructures. These phenomena are generally associated with the presence of ancient underground quarries for the extraction of calcarenite rock, used for building or ornamental materials. These quarries were poorly constructed and abandoned throughout history.
An automatic approach for rill network extraction to measure rill erosion by terrestrial and low‐cost unmanned aerial vehicle photogrammetry
2019
For an erosion event (October 2016) occurred at the Sparacia experimental area (Southern Italy), both terrestrial and low-altitude aerial surveys were carried out by consumer grade camera and quadcopter (low-cost unmanned aerial vehicle [UAV]) to measure rill erosion on two plots with steepness of 22% and 26%. Applying the structure from motion (SfM) technique, the three-dimensional digital terrain models (3D-DTMs) and the quasi three-dimensional models (2.5D-digital elevation model [DEM]) were obtained by the two surveys. Furthermore, 3D-DTM and DEM were built using the available aerial photographs (166) and adding 40 terrestrial photographs. For the first time, the convergence index was a…
Determination of Glyphosate and AMPA in Food Samples Using Membrane Extraction Technique for Analytes Preconcentration
2021
The method for determining glyphosate (NPG) and its metabolite AMPA (aminomethyl phosphonic acid) in solid food samples using UAE-SLM-HPLC–PDA technique was developed. Firstly, ultrasonic-assisted solvent extraction (UAE) and protein precipitation step were used for the analyte isolation. Then, the supernatant was evaporated to dryness and redissolved in distilled water (100 mL). The obtained solution was alkalized to pH 11 (with 1 M NaOH) and used directly as donor phase in SLM (supported liquid membrane) extraction. The SLM extraction was performed using 2 M NaCl (5 mL) as an acceptor phase. The flow rate of both phases (donor and acceptor) was set at 0.2 mL/min. The membrane extraction t…
Determination of Glyphosate and AMPA in Food Samples Using Membrane Extraction Technique for Analytes Preconcentration
2022
The method for determining glyphosate (NPG) and its metabolite AMPA (aminomethyl phosphonic acid) in solid food samples using UAE-SLM-HPLC–PDA technique was developed. Firstly, ultrasonic-assisted solvent extraction (UAE) and protein precipitation step were used for the analyte isolation. Then, the supernatant was evaporated to dryness and redissolved in distilled water (100 mL). The obtained solution was alkalized to pH 11 (with 1 M NaOH) and used directly as donor phase in SLM (supported liquid membrane) extraction. The SLM extraction was performed using 2 M NaCl (5 mL) as an acceptor phase. The flow rate of both phases (donor and acceptor) was set at 0.2 mL/min. The membrane extraction t…
Supported liquid membrane extraction ofglyphosate metabolites
2001
Use of the supported liquid membrane (SLM) technique for (aminomethyl)phosphonic acid (AMPA) extraction is presented. For the extraction of this analyte a suitable SLM system involves a liquid membrane containing Aliquat 336 – a cationic carrier that facilitates AMPA transport. The extraction of this compound, as in the case of glyphosate, is dependent on the donor phase pH and the concentration and type of counter‐ion in the acceptor phase, although some differences are also observed. In both cases the transport mechanism is counter‐coupled transport in which the driving force of mass transport over the membrane is created by the gradient of chloride anions from the acceptor to donor phase.
The Application of Supercritical Fluids Technology to Recover Healthy Valuable Compounds from Marine and Agricultural Food Processing By-Products: A …
2021
Food by-products contain a remarkable source of bioactive molecules with many benefits for humans; therefore, their exploitation can be an excellent opportunity for the food sector. Moreover, the revalorization of these by-products to produce value-added compounds is considered pivotal for sustainable growth based on a circular economy. Traditional extraction technologies have several drawbacks mainly related to the consumption of hazardous organic solvents, and the high temperatures maintained for long extraction periods which cause the degradation of thermolabile compounds as well as a low extraction efficiency of desired compounds. In this context, supercritical fluid extraction (SFE) ha…