0000000000026540
AUTHOR
Aku Suhonen
Effect of a Rigid Sulfonamide Bond on Molecular Folding: A Case Study
A disulfonamide compound with bulky aromatic side chains was prepared, and its properties as a potential building block for foldamers were evaluated. Two different solvate crystal forms of the compound were identified and compared to the structures of an analogous oligoamide and related disulfonamides. The disulfonamide is unfolded in one of the solvates, whereas in the other one, a loosely folded conformer stabilized by an intramolecular hydrogen bond is found. Density functional calculations indicated that the loosely folded conformer is slightly more stable than its unfolded isomer. The calculations also identified a third, more tightly folded and more extensively hydrogen bonded, confor…
Structural analysis of two foldamer-type oligoamides – the effect of hydrogen bonding on solvate formation, crystal structures and molecular conformation
Author's Final draft The crystal structures and molecular conformations of two foldamer-type oligoamides were analyzed. One polymorphic form and seven solvates were found for N¹,N³-bis(2-benzamidophenyl)benzene-1,3-dicarboxamide (the benzene variant), and two polymorphic forms and six solvates for N²,N⁶-bis(2-benzamidophenyl)pyridine-2,6-dicarboxamide (the pyridine variant). Three crystal structures of the benzene variant and seven structures of the pyridine variant were solved using single crystal X-ray diffraction. The crystal structures showed that the different modes of intramolecular hydrogen bonding strongly affect the conformation and folding of the molecules, which is most evidently…
Conformational properties and folding analysis of a series of seven oligoamide foldamers
33 crystal structures (11 unsolvated and 22 solvates) of a series of seven oligoamide foldamers were analysed. The crystal structures revealed that despite the structural and environmental differences the series of foldamers prefer only two general conformations, a protohelical @-conformation and a sigmoidal S-conformation. Both conformations also have preferred crystal packing motifs and solvate forming tendencies. Hydrogen bonding was found to be the most decisive factor in conformational preference, but steric properties, the type of the peripheral substituents, as well as solvent and aromatic interactions were also found to have an effect on the conformational details and crystal form. …
The Missing Member of the Partially O-Alkylated Resorcinarene Family: Synthesis and Conformation of Methyl Tetramethoxy Resorcinarene
An improved Lewis acid catalyzed synthesis method for methyl tetramethoxy resorcinarene is described, which produced the missing lower rim methyl derivative of this partially O-alkylated resorcinarene family. Structural characterization by means of variable temperature NMR experiments and single crystal X-ray diffraction studies furthermore revealed that the resorcinarene core adopts different conformations in the solid state and in solution. peerReviewed
Oligoamide Foldamers as Helical Chloride Receptors-the Influence of Electron-Withdrawing Substituents on Anion-Binding Interactions.
The anion-binding properties of three closely related oligoamide foldamers were studied using NMR spectroscopy, isothermal titration calorimetry and mass spectrometry, as well as DFT calculations. The 1 H NMR spectra of the foldamers in [D6 ]acetone solution revealed partial preorganization by intramolecular hydrogen bonding, which creates a suitable cavity for anion binding. The limited size of the cavity, however, enabled efficient binding by the inner amide protons only for the chloride anion resulting in the formation of a thermodynamically stable 1:1 complex. All 1:1 chloride complexes displayed a significant favourable contribution of the entropy term. Most likely, this is due to the …
Cation binding resorcinarene bis-crowns: the effect of lower rim alkyl chain length on crystal packing and solid lipid nanoparticles
A group of seven resorcinarene bis-crown ethers (CNBC5) with two polyether bridges at the upper rim and either propyl, butyl, pentyl, heptyl, nonyl, decyl or undecyl groups at the lower rim were synthesized and their binding properties with Cs+ were investigated by NMR titration. The bis-crowns form 1:2 complexes with Cs+ with binding constants of logK 4–5. Crystal structures of bis-crowns and their Cs+ and K+ complexes were studied and different packing motifs were found depending on the alkyl chain length. Short ethyl, propyl and butyl alkyl chains gave a layer or pillar packing where the polar and non-polar regions cannot be distinguished, whereas longer pentyl and decyl chains formed bi…
Supramolecular chirality and symmetry breaking of fluoride complexes of achiral foldamers
Aromatic oligoamide foldamers containing a central pyridine-2,6-dicarbonyl motif are partially preorganized to favor the binding of fluoride anions. In the solid state, the foldamer-fluoride complexes form achiral, polar and chiral crystal structures depending on the chemical structure of the foldamer. One of the six foldamers studied here, a C2v symmetrical foldamer (1), formed repeatedly chiral crystal structures when crystallized with tetra-butylammonium fluoride, showing supramolecular bulk chirality and symmetry breaking in crystallization.
Orgaanisten yhdisteiden kiinteän tilan rakennemääritysmenetelmät
Pro gradu -tutkielmassa käydään läpi 16 yleistä orgaanisten yhdisteiden kiinteän tilan rakennemääritysmenetelmää. Erityistä huomiota on tutkielmassa osoitettu röntgendiffraktiolle, kiinteän tilan NMR-spektroskopialle ja infrapunaspektroskopialle. Erikoistyössä valmistettiin kaksi uutta amidofoldameeriä ja yksi uusi sulfonyylifoldameeri. Valmistettujen yhdisteiden ominaisuuksia tutkittiin ja niitten rakenteet määritettiin. Lisäksi määritettiin yhden muodostetun fluorikompleksin rakenne.
Oligoamide Foldamers as Helical Chloride Receptors : the Influence of Electron-Withdrawing Substituents on Anion-Binding Interactions
The anion‐binding properties of three closely related oligoamide foldamers were studied using NMR spectroscopy, isothermal titration calorimetry and mass spectrometry, as well as DFT calculations. The 1H NMR spectra of the foldamers in [D6]acetone solution revealed partial preorganization by intramolecular hydrogen bonding, which creates a suitable cavity for anion binding. The limited size of the cavity, however, enabled efficient binding by the inner amide protons only for the chloride anion resulting in the formation of a thermodynamically stable 1:1 complex. All 1:1 chloride complexes displayed a significant favourable contribution of the entropy term. Most likely, this is due to the re…
Folding Patterns in a Family of Oligoamide Foldamers
A series of small, unsymmetrical pyridine-2,6-dicarboxylamide oligoamide foldamers with varying lengths and substituents at the end groups were synthetized to study their conformational properties and folding patterns. The @-type folding pattern resembled the oxyanion-hole motifs of enzymes, but several alternative folding patterns could also be characterized. Computational studies revealed several alternative conformers of nearly equal stability. These folding patterns differed from each other in their intramolecular hydrogen-bonding patterns and aryl-aryl interactions. In the solid state, the foldamers adopted either the globular @-type fold or the more extended S-type conformers, which w…
Solid state conformational behavior and interactions of a series of aromatic oligoamide foldamers
The topic of this thesis is aromatic oligoamide foldamers. The literary review of the thesis discusses the general features of foldamers and their design and then focuses on the specific examples of aromatic oligoamide foldamers. The experimental part of the thesis discusses the design and preparation of a family of aromatic oligoamide foldamers that can adopt a helical conformation. The folding is directed by intramolecular hydrogen bonding and stabilized by intramolecular aromatic interactions. The focus of the thesis is the analysis of the solid state conformations of ten foldamer analogues. The analysis is based on forty different crystal structures which are determined using single cry…
Structural Tuning and Conformational Stability of Aromatic Oligoamide Foldamers
A series of aromatic oligoamide foldamers with two or three pyridine-2,6-dicarboxamide units as their main folding motifs and varying aromatic building blocks as linkers have been synthetized to study the effects of the structural variation on the folding properties and conformational stability. Crystallographic studies showed that in the solid state the central linker unit either elongates the helices and more open S-shaped conformations, compresses the helices to more compact conformations or acts as a rigid spacer separating the pyridine-2,6-dicarboxamide units, which for their part add the predictability of the conformational properties. Multidimensional NMR studies showed that, even in…
CCDC 1555247: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1436660: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1436663: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1438546: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 919270: Experimental Crystal Structure Determination
Related Article: Tiia-Riikka Tero, Aku Suhonen, Kirsi Salorinne, Hélène Campos-Barbosa, Maija Nissinen|2013|Org.Lett.|15|1096|doi:10.1021/ol400118t
CCDC 1038219: Experimental Crystal Structure Determination
Related Article: Minna Kortelainen, Aku Suhonen, Andrea Hamza, Imre Pápai, Elisa Nauha, Sanna Yliniemelä-Sipari, Maija Nissinen, Petri M. Pihko|2015|Chem.-Eur.J.|21|9493|doi:10.1002/chem.201406521
CCDC 1022891: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Ian S. Morgan, Elisa Nauha, Kaisa Helttunen, Heikki M. Tuononen, Maija Nissinen|2015|Cryst.Growth Des.|15|2602|doi:10.1021/acs.cgd.5b00424
CCDC 1038222: Experimental Crystal Structure Determination
Related Article: Minna Kortelainen, Aku Suhonen, Andrea Hamza, Imre Pápai, Elisa Nauha, Sanna Yliniemelä-Sipari, Maija Nissinen, Petri M. Pihko|2015|Chem.-Eur.J.|21|9493|doi:10.1002/chem.201406521
CCDC 1552171: Experimental Crystal Structure Determination
Related Article: Kaisa Helttunen, Riia Annala, Aku Suhonen, Elisa Nauha, Juha Linnanto, Maija Nissinen|2017|CrystEngComm|19|5184|doi:10.1039/C7CE01109A
CCDC 1038221: Experimental Crystal Structure Determination
Related Article: Minna Kortelainen, Aku Suhonen, Andrea Hamza, Imre Pápai, Elisa Nauha, Sanna Yliniemelä-Sipari, Maija Nissinen, Petri M. Pihko|2015|Chem.-Eur.J.|21|9493|doi:10.1002/chem.201406521
CCDC 1022892: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Ian S. Morgan, Elisa Nauha, Kaisa Helttunen, Heikki M. Tuononen, Maija Nissinen|2015|Cryst.Growth Des.|15|2602|doi:10.1021/acs.cgd.5b00424
CCDC 1436674: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1555255: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1555258: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1552172: Experimental Crystal Structure Determination
Related Article: Kaisa Helttunen, Riia Annala, Aku Suhonen, Elisa Nauha, Juha Linnanto, Maija Nissinen|2017|CrystEngComm|19|5184|doi:10.1039/C7CE01109A
CCDC 1436667: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1552170: Experimental Crystal Structure Determination
Related Article: Kaisa Helttunen, Riia Annala, Aku Suhonen, Elisa Nauha, Juha Linnanto, Maija Nissinen|2017|CrystEngComm|19|5184|doi:10.1039/C7CE01109A
CCDC 1436665: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1552175: Experimental Crystal Structure Determination
Related Article: Kaisa Helttunen, Riia Annala, Aku Suhonen, Elisa Nauha, Juha Linnanto, Maija Nissinen|2017|CrystEngComm|19|5184|doi:10.1039/C7CE01109A
CCDC 1555253: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 919269: Experimental Crystal Structure Determination
Related Article: Tiia-Riikka Tero, Aku Suhonen, Kirsi Salorinne, Hélène Campos-Barbosa, Maija Nissinen|2013|Org.Lett.|15|1096|doi:10.1021/ol400118t
CCDC 1436670: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 919268: Experimental Crystal Structure Determination
Related Article: Tiia-Riikka Tero, Aku Suhonen, Kirsi Salorinne, Hélène Campos-Barbosa, Maija Nissinen|2013|Org.Lett.|15|1096|doi:10.1021/ol400118t
CCDC 1038220: Experimental Crystal Structure Determination
Related Article: Minna Kortelainen, Aku Suhonen, Andrea Hamza, Imre Pápai, Elisa Nauha, Sanna Yliniemelä-Sipari, Maija Nissinen, Petri M. Pihko|2015|Chem.-Eur.J.|21|9493|doi:10.1002/chem.201406521
CCDC 1038217: Experimental Crystal Structure Determination
Related Article: Minna Kortelainen, Aku Suhonen, Andrea Hamza, Imre Pápai, Elisa Nauha, Sanna Yliniemelä-Sipari, Maija Nissinen, Petri M. Pihko|2015|Chem.-Eur.J.|21|9493|doi:10.1002/chem.201406521
CCDC 1555260: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1555245: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1436669: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1022889: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Ian S. Morgan, Elisa Nauha, Kaisa Helttunen, Heikki M. Tuononen, Maija Nissinen|2015|Cryst.Growth Des.|15|2602|doi:10.1021/acs.cgd.5b00424
CCDC 1555251: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1436668: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1022890: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Ian S. Morgan, Elisa Nauha, Kaisa Helttunen, Heikki M. Tuononen, Maija Nissinen|2015|Cryst.Growth Des.|15|2602|doi:10.1021/acs.cgd.5b00424
CCDC 1436662: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1552173: Experimental Crystal Structure Determination
Related Article: Kaisa Helttunen, Riia Annala, Aku Suhonen, Elisa Nauha, Juha Linnanto, Maija Nissinen|2017|CrystEngComm|19|5184|doi:10.1039/C7CE01109A
CCDC 1552174: Experimental Crystal Structure Determination
Related Article: Kaisa Helttunen, Riia Annala, Aku Suhonen, Elisa Nauha, Juha Linnanto, Maija Nissinen|2017|CrystEngComm|19|5184|doi:10.1039/C7CE01109A
CCDC 1436673: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1038216: Experimental Crystal Structure Determination
Related Article: Minna Kortelainen, Aku Suhonen, Andrea Hamza, Imre Pápai, Elisa Nauha, Sanna Yliniemelä-Sipari, Maija Nissinen, Petri M. Pihko|2015|Chem.-Eur.J.|21|9493|doi:10.1002/chem.201406521
CCDC 1038223: Experimental Crystal Structure Determination
Related Article: Minna Kortelainen, Aku Suhonen, Andrea Hamza, Imre Pápai, Elisa Nauha, Sanna Yliniemelä-Sipari, Maija Nissinen, Petri M. Pihko|2015|Chem.-Eur.J.|21|9493|doi:10.1002/chem.201406521
CCDC 1436659: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 919271: Experimental Crystal Structure Determination
Related Article: Tiia-Riikka Tero, Aku Suhonen, Kirsi Salorinne, Hélène Campos-Barbosa, Maija Nissinen|2013|Org.Lett.|15|1096|doi:10.1021/ol400118t
CCDC 1555256: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1436672: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1555244: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1555248: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1555250: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1555259: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1555249: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1436666: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1038215: Experimental Crystal Structure Determination
Related Article: Minna Kortelainen, Aku Suhonen, Andrea Hamza, Imre Pápai, Elisa Nauha, Sanna Yliniemelä-Sipari, Maija Nissinen, Petri M. Pihko|2015|Chem.-Eur.J.|21|9493|doi:10.1002/chem.201406521
CCDC 1038218: Experimental Crystal Structure Determination
Related Article: Minna Kortelainen, Aku Suhonen, Andrea Hamza, Imre Pápai, Elisa Nauha, Sanna Yliniemelä-Sipari, Maija Nissinen, Petri M. Pihko|2015|Chem.-Eur.J.|21|9493|doi:10.1002/chem.201406521
CCDC 1552169: Experimental Crystal Structure Determination
Related Article: Kaisa Helttunen, Riia Annala, Aku Suhonen, Elisa Nauha, Juha Linnanto, Maija Nissinen|2017|CrystEngComm|19|5184|doi:10.1039/C7CE01109A
CCDC 1552176: Experimental Crystal Structure Determination
Related Article: Kaisa Helttunen, Riia Annala, Aku Suhonen, Elisa Nauha, Juha Linnanto, Maija Nissinen|2017|CrystEngComm|19|5184|doi:10.1039/C7CE01109A
CCDC 1436664: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1555254: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1436671: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1436661: Experimental Crystal Structure Determination
Related Article: Aku Suhonen, Minna Kortelainen, Elisa Nauha, Sanna Yliniemelä-Sipari, Petri M. Pihko, Maija Nissinen|2016|CrystEngComm|18|2005|doi:10.1039/C5CE02458G
CCDC 1555252: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1555257: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1555246: Experimental Crystal Structure Determination
Related Article: Riia Annala, Aku Suhonen, Heikki Laakkonen, Perttu Permi, Maija Nissinen|2017|Chem.-Eur.J.|23|16671|doi:10.1002/chem.201703985
CCDC 1455102: Experimental Crystal Structure Determination
WAFYAG : N,N'-(((1,3-phenylenedisulfonyl)bis(azanediyl))bis(2,1-phenylene))dibenzamide perdeuteroacetone solvate Space Group: C2/c, Cell: a 24.9217(15)Å b 6.9550(5)Å c 20.6193(15)Å, α 90° β 105.782(7)° γ 90°. Work published 2016 via Cambridge Crystallographic Data Centre.