0000000000060984
AUTHOR
M. Siitari-kauppi
Characterizing Low-Permeable Granitic Rock from Micrometer to Centimeter Scale: X-ray Microcomputed Tomography, Confocal Laser Scanning Microscopy and 14C-PMMA Method
AbstractFirst results of combining X-ray microcomputer tomography (µCT), confocal laser-scanning microscopy (CLSM) and 14C-polymethylmethacrylate (14C-PMMA) impregnation techniques in the study of granitic rock samples are reported. Combining results of µCT and CLSM with those of the 14C-PMMA technique, the mineral-specific porosity and morphology of the open pore space, as well as its connectivity, could be analyzed from a micrometer up to a decimeter scale.Three different types of granite were studied. In two cases part of the micro-fissure and pore apertures were found to be in a micrometer scale, but in one case all grain-boundary openings were below the detection limit. Micrometer-scal…
Imaging connected porosity of crystalline rock by contrast agent-aided X-ray microtomography and scanning electron microscopy
We set out to study connected porosity of crystalline rock using X‐ray microtomography and scanning electron microscopy with energy dispersive X‐ray spectroscopy (SEM‐EDS) with caesium chloride as a contrast agent. Caesium is an important radionuclide regarding the final deposition of nuclear waste and also forms dense phases that can be readily distinguished by X‐ray microtomography and SEM‐EDS. Six samples from two sites, Olkiluoto (Finland) and Grimsel (Switzerland), where transport properties of crystalline rock are being studied in situ, were investigated using X‐ray microtomography and SEM‐EDS. The samples were imaged with X‐ray microtomography, immersed in a saturated caesium chlorid…
Pore-space characterization of an altered tonalite by X-ray computed microtomography and the14C-labeled-polymethylmethacrylate method
[1] The structure of geological materials strongly affects migration processes that take place in them and are also important in their weathering and alteration processes. Further information of that structure will also be important for many applications that involve geological materials. The emphasis of this study was thus to characterize the pore structure and porosity of altered tonalite by combining different measuring techniques: X-ray tomography, the14C-polymethylmethacrylate method, electron microscopy, and argon pycnometry. Intragranular porosities were determined using chemical staining of rock surfaces. Three-dimensional distributions of minerals and porosities were evaluated with…