Author: Bao-hua Xu

0000000000076294

AUTHOR

Bao-hua Xu

Zirconocene complexes bearing novel 3-dimethylamino-1,2-dihydropentalene derived ligand systems.

Coupling of the N,N-dimethylacrylamides 6a-c with cyclopentadienide resulted in the formation of the substituted 3-dimethylamino-1,2-dihydropentalnenes 2a-c. Deprotonation followed by metallation with CpZrCl(3)·DME gave the substituted zirconocenes 12a-c. The reaction of 3-dimethylamino-1-methyl-dihydropentalene 2a with ZrCl(2)(NMe(2))(2)·2THF resulted in a unique coupling between a pair of the aminodihydropentalene derivatives to yield an unsymmetrically bridged novel ansa-zirconocene framework (9a). Treatment of the 1,1-dimethyl-substituted substrate 2b with this Zr-amido reagent in contrast resulted in a clean deprotonation and formation of the unbridged bis(dimethylaminohydropentalenyl)…

research product

CCDC 778228: Experimental Crystal Structure Determination

Related Article: Bao-Hua Xu, G.Kehr, R.Frohlich, E.Nauha, G.Erker|2010|Dalton Trans.|39|9973|doi:10.1039/c0dt00515k

research product

CCDC 778229: Experimental Crystal Structure Determination

Related Article: Bao-Hua Xu, G.Kehr, R.Frohlich, E.Nauha, G.Erker|2010|Dalton Trans.|39|9973|doi:10.1039/c0dt00515k

research product

CCDC 778226: Experimental Crystal Structure Determination

Related Article: Bao-Hua Xu, G.Kehr, R.Frohlich, E.Nauha, G.Erker|2010|Dalton Trans.|39|9973|doi:10.1039/c0dt00515k

research product

CCDC 778227: Experimental Crystal Structure Determination

Related Article: Bao-Hua Xu, G.Kehr, R.Frohlich, E.Nauha, G.Erker|2010|Dalton Trans.|39|9973|doi:10.1039/c0dt00515k

research product

CCDC 778230: Experimental Crystal Structure Determination

Related Article: Bao-Hua Xu, G.Kehr, R.Frohlich, E.Nauha, G.Erker|2010|Dalton Trans.|39|9973|doi:10.1039/c0dt00515k

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PEPhysical Sciences and Engineering
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