Zircon M257 - a homogeneous natural reference material for the ion microprobe U-Pb analysis of zircon
We introduce and propose zircon M257 as a future reference material for the determination of zircon U-Pb ages by means of secondary ion mass spectrometry. This light brownish, flawless, cut gemstone specimen from Sri Lanka weighed 5.14 g (25.7 carats). Zircon M257 has TIMS-determined, mean isotopic ratios (2s uncertainties) of 0.09100 ± 0.00003 for 206pb/238U and 0.7392 ± 0.0003 for 207pb/235U. Its 206pb/238U age is 561.3 ± 0.3 Ma (unweighted mean, uncertainty quoted at the 95% confidence level); the U-Pb system is concordant within uncertainty of decay constants. Zircon M257 contains ∼ 840 μg g−1 U (Th/U ∼ 0.27). The material exhibits remarkably low heterogeneity, with a virtual absence of…
Zircon M127 - A Homogeneous Reference Material for SIMS U-Pb Geochronology Combined with Hafnium, Oxygen and, Potentially, Lithium Isotope Analysis
Faculty of Geosciences, Geography and Astronomy, University of Vienna; Beijing SHRIMP Centre, Chinese Academy of Geological Sciences; European Commission [MEXC-CT-2005-024878]; FWF Austrian Science Fund [P20028-N10, P24448-N19]; U.S. National Science Foundation [EAR 1524336]
Incomplete retention of radiation damage in zircon from Sri Lanka
A suite of 18 zircon gemstones from placers in the Highland/Southwestern Complex, Sri Lanka, were subjected to a comprehensive study of their radiation damages and ages. The investigation included X-ray diffraction, Raman and PL spectroscopy, electron microprobe, PIXE and HRTEM analysis, as well as (U-Th)/He and SHRIMP U-Th-Pb age determinations. Zircon samples described in this study are virtually homogeneous. They cover the range from slightly metamict to nearly amorphous. Generally concordant U-Th-Pb ages averaging 555 ± 11 Ma were obtained. Late Ordovician zircon (U-Th)/He ages scattering around 443 ± 9 Ma correspond reasonably well with previously determined biotite Rb-Sr ages for rock…
Linking growth episodes of zircon and metamorphic textures to zircon chemistry: an example from the ultrahigh-temperature granulites of Rogaland (SW Norway)
In-situ U-Th-Pb analyses by ion-microprobe on zircon in intact textural relationships are combined with backscatter and cathodoluminescence imaging and trace element analyses to provide evidence for growth episodes of zircon. This approach helps: (a) to unravel the polymetamorphic history of aluminous migmatitic and granitoid gneisses of the regional contact aureole around the Rogaland anorthosite-norite intrusive complex; and (b) to constrain the age of M 2 ultrahigh-temperature (UHT) metamorphism and the subsequent retrograde M 3 event. All samples yield magmatic inherited zircon of c. 1035 Ma, some an additional group at c. 1050 Ma. This suggests that loss of Pb by volume diffusion in no…