Author: Liene Anteina

0000000000308930

AUTHOR

Liene Anteina

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ChemInform Abstract: Dialkylimidazolium Dimethyl Phosphates as Solvents and Catalysts for the Knoevenagel Condensation Reaction.

2014

Knoevenagel condensation between benzaldehyde and ethyl cyanoacetate in the presence of an equimolar amount of 1,3-dialkylimidazolium dimethyl phosphate ionic liquids is investigated.

Benzaldehydechemistry.chemical_compoundchemistryEthyl cyanoacetateIonic liquidOrganic chemistryKnoevenagel condensationGeneral MedicineCondensation reactionPhosphateCatalysisChemInform

researchProduct

Dialkylimidazolium dimethyl phosphates as solvents and catalysts for the Knoevenagel condensation reaction

2014

Abstract The reaction between benzaldehyde and ethyl cyanoacetate is investigated in 1,3-dialkylimidazolium salts as solvents. The impact of both ions in these ionic liquids on the yield of the condensation reaction product is examined. Potentiometric titrations are employed for quantitative analyses of the best ionic liquids, revealing these to be 1,3-dialkylimidazolium dimethyl phosphates.

Organic ChemistryPotentiometric titrationCondensation reactionBiochemistryCatalysisIonBenzaldehydechemistry.chemical_compoundchemistryYield (chemistry)Drug DiscoveryIonic liquidOrganic chemistryKnoevenagel condensationTetrahedron Letters

researchProduct

Kondensācijas reakcijas imidazolija dialkilfosfātu vidē

2012

Darba literatūras apskata daļā ietverta vispārīga informācija par jonu šķidrumu iegūšanu, to uzbūvi un īpašībām, kā arī apkopota literatūra par jonu šķidrumu izmantošanas iespējām kondensāciju reakciju veikšanai. Laboratorijā veikta imidazolija dialkilfosfātu rindas jonu šķidrumu iegūšana, un iegūto savienojuma struktūras pierādītas ar 1H KMR spektroskopijas metodi. Noteikti svarīgākie jonu šķidrumu raksturlielumi – ūdens saturs, termiskā stabilitāte, polaritāte un jonu šķidrumu ūdens šķīdumu pH. Iegūtajos jonu šķidrumos veiktas kondensāciju reakcijas un raksturota to ietekme uz reakcijas produktu iznākumiem.

researchProduct

PEPhysical Sciences and Engineering
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