0000000000323541

AUTHOR

I. Nakurte

showing 1 related works from this author

Ultra high performance liquid chromatography-time-of-flight high resolution mass spectrometry in the analysis of hexabromocyclododecane diastereomers…

2014

An efficient ultra high performance liquid chromatography (UHPLC)-time-of-flight high resolution mass spectrometry (TOF-HRMS) method was elaborated for the determination of hexabromocyclododecane (HBCD) diastereomers in fish samples and compared against UHPLC-Orbitrap-HRMS and UHPLC-triple quadrupole (QqQ) tandem MS (MS/MS) techniques. The TOF-HRMS analyzer was operated at high resolution (>10000 full width at half maximum (FWHM)) with scanning the m/z range from 600 to 700, to achieve picogram quantitation limits. The effects of various operational parameters on the instrumental response were systematically investigated. Evaluation of the influence of sample clean-up procedure steps on sig…

Analytical chemistryTandem mass spectrometryOrbitrapBiochemistryMass SpectrometryAnalytical Chemistrylaw.inventionMatrix (chemical analysis)Gel permeation chromatographychemistry.chemical_compoundColumn chromatographylawTandem Mass SpectrometryAnimalsMuscle SkeletalChromatography High Pressure LiquidHexabromocyclododecaneChromatographyEelsOrganic ChemistryFishesReproducibility of ResultsGeneral MedicineRepeatabilityTriple quadrupole mass spectrometerHydrocarbons BrominatedchemistryWater Pollutants ChemicalEnvironmental MonitoringJournal of chromatography. A
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