0000000000368158

AUTHOR

David Julian Mcclements

showing 2 related works from this author

Influence of lipid physical state on the in vitro digestibility of emulsified lipids.

2008

The objective of this study was to investigate the influence of the physical state of emulsified lipids on their in vitro digestibility by pancreatic lipase. A 10 wt % tripalmitin oil-in-water emulsion stabilized by sodium dodecyl sulfate (0.9 wt % SDS) was prepared at a temperature (>70 degrees C) above the melting point of the lipid phase (T(m) approximately 60 degrees C). A portion of this emulsion was cooled to a temperature (0 degrees C for 15 min) well below the crystallization temperature of the emulsified lipid (T(c) approximately 22 degrees C) and then warmed to 37 degrees C so as to have completely solid lipid particles. Another portion of the emulsion was directly cooled from 70 …

Chemical PhenomenaSwineFatty Acids NonesterifiedIn Vitro Techniqueschemistry.chemical_compoundAnimalsLipaseSodium dodecyl sulfateParticle SizeChromatographybiologyChemistry PhysicalLipid metabolismGeneral ChemistryLipaseLipid MetabolismLipidschemistryEmulsionTripalmitinbiology.proteinDigestionEmulsionsLipid particleParticle sizeGeneral Agricultural and Biological SciencesLipid digestionJournal of agricultural and food chemistry
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Simultaneous determination of four 5-hydroxy polymethoxyflavones by reversed-phase high performance liquid chromatography with electrochemical detect…

2009

Accumulating evidence has suggested the potential health-promoting effects of 5-hydroxy polymethoxyflavones (5-OH-PMFs) naturally existing in citrus genus. However, research efforts are hampered by the lack of reliable and sensitive methods for their determination in plant materials and biological samples. Using reversed-phase high performance liquid chromatography (HPLC) equipped with electrochemical (EC) detection, we have developed a fast and highly sensitive method for quantification of four 5-OH-PMFs, namely 5-hydroxy-6,7,8,3',4'-pentamethoxyflavone, 5-hydroxy-3,6,7,8,3',4'-hexamethoxyflavone, 5-hydroxy-6,7,4'-trimethoxyflavone, and 5-hydroxy-6,7,8,4'-tetramethoxyflavone. The method wa…

FlavonoidsDetection limitOrange juicechemistry.chemical_classificationCitrusAccuracy and precisionChromatographyOrganic ChemistryFlavonoidReproducibility of ResultsElectrochemical TechniquesGeneral MedicineReversed-phase chromatographyElectrochemical detectionHydrogen-Ion ConcentrationFlavonesSensitivity and SpecificityBiochemistryHigh-performance liquid chromatographyAnalytical ChemistryBeverageschemistryLinear ModelsChromatography High Pressure LiquidCitrus × sinensisJournal of Chromatography A
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