0000000000459847

AUTHOR

Michael Serafin

showing 4 related works from this author

Selective Preparation of Diamondoid Phosphonates

2014

We present an effective sequence for the preparation of phosphonic acid derivatives of the diamondoids diamantane, triamantane, [121]tetramantane, and [1(2,3)4]pentamantane. The reactions of the corresponding diamondoid hydroxy derivatives with PCl3 in sulfuric or trifluoroacetic acid give mono- as well as didichlorophosphorylated diamondoids in high preparative yields.

Phosphonic acid derivativeschemistry.chemical_compoundchemistryOrganic ChemistryTrifluoroacetic acidOrganic chemistrySequence (biology)DiamondoidDiamantaneThe Journal of Organic Chemistry
researchProduct

CCDC 1009244: Experimental Crystal Structure Determination

2014

Related Article: Andrey A. Fokin, Raisa I. Yurchenko, Boryslav A. Tkachenko, Natalie A. Fokina, Maria A. Gunawan, Didier Poinsot, Jeremy E. P. Dahl , Robert M. K. Carlson , Michael Serafin , Hélène Cattey, Jean-Cyrille Hierso , and Peter R. Schreiner|2014|J.Org.Chem.|79|5369|doi:10.1021/jo500793m

Space GroupCrystallographyCrystal Systemnonacyclo[11.7.1.1^618^.0^116^.0^211^.0^38^.0^419^.0^817^.0^1015^]docos-6-ylphosphonic dichlorideCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 1009245: Experimental Crystal Structure Determination

2014

Related Article: Andrey A. Fokin, Raisa I. Yurchenko, Boryslav A. Tkachenko, Natalie A. Fokina, Maria A. Gunawan, Didier Poinsot, Jeremy E. P. Dahl , Robert M. K. Carlson , Michael Serafin , Hélène Cattey, Jean-Cyrille Hierso , and Peter R. Schreiner|2014|J.Org.Chem.|79|5369|doi:10.1021/jo500793m

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameterspentacyclo[7.3.1.1^412^.0^27^.0^611^]tetradec-1-ylphosphonic dichlorideExperimental 3D Coordinates
researchProduct

CCDC 1009243: Experimental Crystal Structure Determination

2014

Related Article: Andrey A. Fokin, Raisa I. Yurchenko, Boryslav A. Tkachenko, Natalie A. Fokina, Maria A. Gunawan, Didier Poinsot, Jeremy E. P. Dahl , Robert M. K. Carlson , Michael Serafin , Hélène Cattey, Jean-Cyrille Hierso , and Peter R. Schreiner|2014|J.Org.Chem.|79|5369|doi:10.1021/jo500793m

Space GroupCrystallographyCrystal SystemCrystal Structureundecacyclo[9.9.1.1^113^.1^37^.1^319^.1^59^.1^515^.0^29^.0^417^.0^1325^.0^1724^]hexacos-7-ylphosphonic dichlorideCell ParametersExperimental 3D Coordinates
researchProduct