0000000000470936

AUTHOR

I. Fedosov

showing 4 related works from this author

1H, 13C, 15N NMR, ESI mass spectral and single crystal X-ray structural characterization of three spiro[pyrrolidine-2,3′-oxindoles]

2006

Abstract Three spiro[pyrrolidine-2,3′-oxindoles], 1,1′,2,2′,5′,6′,7′,7′a-octahydro-2-oxo-1′-phenyl-spiro[3H-indole-3,3′-[3H]-pyrrolizine]-2′-carboxylic acid methyl ester (1), 1,1′,2,2′,5′,6′,7′,7′a-octahydro-2-oxo-1′-nitro-2′-phenyl-spiro[3H-indole-3, 3′-[3H]-pyrrolizine] (2) and 1,1′,2,2′,5′,6′,7′,7′a-octahydro-2-oxo-1′-nitro-2′-(4″-chlorophenyl)-spiro[3H-indole-3,3′-[3H]-pyrrolizine] (3) have been synthesized and their 1H, 13C and 15N spectra assigned. The chemical shift assignments are based on Pulsed Field Gradient (PFG) Double Quantum Filter (DQF) 1H, 1H correlation spectroscopy (COSY), PFG 1H, 13C Heteronuclear Multiple Quantum Coherence (HMQC) and PFG 1H,X (X = 13C and 15N) Heteronuc…

Chemical shiftOrganic ChemistryAnalytical chemistryPyrrolidineSpectral lineAnalytical ChemistryInorganic Chemistrychemistry.chemical_compoundCrystallographychemistryHeteronuclear moleculePulsed field gradientTwo-dimensional nuclear magnetic resonance spectroscopySingle crystalSpectroscopyMonoclinic crystal systemJournal of Molecular Structure
researchProduct

CCDC 289303: Experimental Crystal Structure Determination

2007

Related Article: K.Laihia, A.Valkonen, E.Kolehmainen, A.Antonov, D.Zhukov, I.Fedosov, V.Nikiforov|2006|J.Mol.Struct.|800|100|doi:10.1016/j.molstruc.2006.03.095

11'22'5'6'7'7a'-octahydro-2-oxo-1'-nitro-2'-(4''-chlorophenyl)-spiro(3H-indole-33'-(3H)-pyrrolizine)Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
researchProduct

CCDC 289301: Experimental Crystal Structure Determination

2007

Related Article: K.Laihia, A.Valkonen, E.Kolehmainen, A.Antonov, D.Zhukov, I.Fedosov, V.Nikiforov|2006|J.Mol.Struct.|800|100|doi:10.1016/j.molstruc.2006.03.095

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersMethyl 11'22'5'6'7'7a'-octahydro-2-oxo-1'-phenyl-spiro(3H-indole-33'-(3H)-pyrrolizine)-2'-carboxylateExperimental 3D Coordinates
researchProduct

CCDC 289302: Experimental Crystal Structure Determination

2007

Related Article: K.Laihia, A.Valkonen, E.Kolehmainen, A.Antonov, D.Zhukov, I.Fedosov, V.Nikiforov|2006|J.Mol.Struct.|800|100|doi:10.1016/j.molstruc.2006.03.095

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters11'22'5'6'7'7a'-octahydro-2-oxo-1'-nitro-2'-phenylspiro(3H-indole-33'-(3H)-pyrrolizine)Experimental 3D Coordinates
researchProduct