0000000000524159

AUTHOR

Niclas Schupp

showing 2 related works from this author

Electrochemical synthesis of carbazoles by dehydrogenative coupling reaction

2020

Abstract A constant current protocol, employing undivided cells, a remarkably low supporting electrolyte concentration, inexpensive electrode materials, and a straightforward precursor synthesis enabling a novel access to N‐protected carbazoles by anodic N,C bond formation using directly generated amidyl radicals is reported. Scalability of the reaction is demonstrated and an easy deblocking of the benzoyl protecting group is presented.

Green chemistry540 Chemistry and allied sciencesDeblocking filterSupporting electrolyteRadicalSustainable Chemistry010402 general chemistryElectrochemistry01 natural sciencesCatalysisCoupling reactionNC couplingProtecting groupgreen chemistry010405 organic chemistryChemistryCommunicationOrganic Chemistryheterocyclic chemistryGeneral ChemistryCombinatorial chemistryCommunications0104 chemical sciencesAnodecarbazoleselectrochemistry540 Chemie
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CCDC 1986341: Experimental Crystal Structure Determination

2020

Related Article: Anton Kehl, Niclas Schupp, Valentina M. Breising, Dieter Schollmeyer, Siegfried R. Waldvogel|2020|Chem.-Eur.J.|26|15847|doi:10.1002/chem.202003430

Space GroupCrystallographyCrystal System(9H-carbazol-9-yl)(phenyl)methanoneCrystal StructureCell ParametersExperimental 3D Coordinates
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