Author: Grazia Principato

0000000001062964

AUTHOR

Grazia Principato

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Resolution of inherently chiral resorcarene derivatives by enantioselective HPLC

1999

Abstract The HPLC enantiomeric resolution of five inherently chiral tetrabenzoxazine derivatives of resorcarenes has been achieved by HPLC using Whelk-Ol and in one case Chiralpak AD as stationary phases. Enantiomeric separation was only observed in a very narrow range of mobile phase compositions. On-column enantiomeric interconversion of a racemic compound with a typical plateau-like elution profile was observed using a Chiralpak AD column

ChromatographyResolution (mass spectrometry)ElutionChemistryOrganic ChemistryDrug DiscoveryNarrow rangeChiralpak ADEnantiomerResorcinareneBiochemistryEnantioselective hplcHigh-performance liquid chromatographyTetrahedron Letters

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