0000000001159389
AUTHOR
J. Picard
Cytoplasmic particles associated with CMS in Faba bean (Vicia faba L.)
International audience
Towards calibration transfer for quantitative analysis of nuclear materials by LIBS
To ensure the quality of their products, manufacturers of nuclear materials currently rely on wet chemistry methods coupled with ICP-MS and ICP-AES. These methods are slow and sometimes hard to implement, which leads the manufacturers to seek new possibilities of online, fast and direct preliminary quality control. Thus, the issue of quantifying metal impurities in both uranium and plutonium matrices by LIBS has been raised. But the lack of calibrated samples and the harsh security constraints hinder any possibility of complete analytical development on these materials. Therefore, we propose a method relying on calibration transfer from several non-nuclear metal matrices to uranium and plut…
Characterization of laser ablation of copper in the irradiance regime of laser-induced breakdown spectroscopy analysis
Abstract The LIBS signal depends both on the ablated mass and on the plasma excitation temperature. These fundamental parameters depend in a complex manner on laser ablation and on laser–plasma coupling. As several works in the literature suggest that laser ablation processes play a predominant role compared to plasma heating phenomena in the LIBS signal variations, this paper focuses on the study of laser ablation. The objective was to determine an interaction regime enabling to maximally control the laser ablation. Nanosecond laser ablation of copper at 266 nm was characterized by scanning electron microscopy and optical profilometry analysis, in air at 1 bar and in the vacuum. The laser …