Author: Jian Hui Ye

0000000001234886

AUTHOR

Jian Hui Ye

showing 2 related works from this author

Semicarbazides as gel forming agents for common solvents and liquid crystals

2006

This paper describes the synthesis of 14 new gelling agents with semicarbazide groups as H-bonding motifs and alkyl- and/or azobenzene side groups. They gel solvents like decaline, 1,2-dichlorobenzene and toluene and liquid crystalline mixtures. X-Ray structure analysis shows that the semicarbazides are connected by H-bonds, each molecule to four neighbours. As a result a ribbon is formed with a core of H-bonded semicarbazide groups and alkyl chains sticking to the side. IR measurements show an unchanged H-bonding motif in large crystals and in the gel fibres, even in LC-mixture. During heating the gel melts (rheology), while the H-bonding motif of the crystal disappears (IR and DSC measure…

chemistry.chemical_classificationSemicarbazideSemicarbazidesStereochemistryInfrared spectroscopyGeneral Chemistrychemistry.chemical_compoundDifferential scanning calorimetryAzobenzenechemistryLiquid crystalPolymer chemistryMaterials ChemistryGlass transitionAlkylJ. Mater. Chem.

researchProduct

CCDC 151383: Experimental Crystal Structure Determination

2006

Related Article: P.Deindorfer, T.Geiger, D.Schollmeyer, Jian Hui Ye, R.Zentel|2006|J.Mater.Chem.|16|351|doi:10.1039/b510474b

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersEthyl 2-((octylamino)carbonyl)hydrazinecarboxylateExperimental 3D Coordinates

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