Author: M. Ezhevskaya

0000000001303498

AUTHOR

M. Ezhevskaya

showing 3 related works from this author

Effect of chelate ring expansion on Jahn-Teller distortion and Jahn-Teller dynamics in copper(II) complexes.

2012

The expanded ligand N,N'-dimethyl-N,N'-dipyridin-2-yl-pyridin-2,6-diamine (ddpd) coordinates to copper(II) ions in a meridional fashion giving the dicationic complex mer-[Cu(ddpd)(2)](BF(4))(2) (1). In the solid state at temperatures below 100 K the cations of 1 localize in Jahn-Teller elongated CuN(6) polyhedra with the longest Cu-N bond pointing in the molecular x or y directions while the z axis is constrained by the tridentate ddpd ligand. The elongated polyhedra are ordered in an antiferrodistortive way giving an idealized zincblende structure. At higher temperature dynamically averaged (fluxional) polyhedra in the molecular x/y directions are observed by multifrequency variable temper…

LigandJahn–Teller effectchemistry.chemical_elementZonal and meridionalOrbital overlapRing (chemistry)Copperlaw.inventionIonInorganic ChemistryCrystallographychemistrylawPhysical and Theoretical ChemistryElectron paramagnetic resonanceInorganic chemistry

researchProduct

CCDC 874635: Experimental Crystal Structure Determination

2013

Related Article: K.Mack, A.W.von Leupoldt, C.Forster, M.Ezhevskaya, D.Hinderberger, K.W.Klinkhammer, K.Heinze|2012|Inorg.Chem.|51|7851|doi:10.1021/ic300929g

mer-bis(NN'-dimethyl-NN'-dipyridin-2-yl-pyridin-26-diamine)-copper(ii) bis(tetrafluoroborate) acetonitrile solvateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 874634: Experimental Crystal Structure Determination

2013

Related Article: K.Mack, A.W.von Leupoldt, C.Forster, M.Ezhevskaya, D.Hinderberger, K.W.Klinkhammer, K.Heinze|2012|Inorg.Chem.|51|7851|doi:10.1021/ic300929g

mer-bis(NN'-dimethyl-NN'-dipyridin-2-yl-pyridin-26-diamine)-copper(ii) bis(tetrafluoroborate) acetonitrile solvateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

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