Author: I. Matera

0000000001308266

AUTHOR

I. Matera

showing 6 related works from this author

Proton and metal binding by cyclen-based highly rigid cryptands.

2010

The basicity properties of the two cryptands L1 and L2, featuring, respectively, a dibenzofuran or a diphenyl ether moiety bridging the 1,7 positions of a 1,4,7,10-tetraazacyclododecane macrocycle (cyclen) have been studied by means of potentiometric, UV-vis and fluorescence emission measurements. Both ligands show a high basicity in the first protonation step, the first basicity constant of L1 being too high to be measured in aqueous solution. The crystal structure of {[HL1]L1}(+) shows that the NH(2)(+) group is involved in an intramolecular hydrogen bonding network, which justifies the observed high basicity in solution. (1)H, (13)C NMR, UV-vis and fluorescence emission measurements show…

Inorganic ChemistryCrystallographychemistry.chemical_compoundAqueous solutionCyclenLigandHydrogen bondChemistryInorganic chemistryCryptandPotentiometric titrationMoietyProtonationDalton transactions (Cambridge, England : 2003)

researchProduct

CCDC 787307: Experimental Crystal Structure Determination

2011

Related Article: C.Bazzicalupi, A.Bencini, S.Ciattini, F.Denat, P.Desogere, C.Goze, I.Matera, B.Valtancoli|2010|Dalton Trans.|39|11643|doi:10.1039/c0dt00948b

Space GroupCrystallographyCrystal System(10-(17-(22'-(Diphenyl ether)dimethyl))-4-azonia-1710-diaza-cyclododecane)-trichloro-zinc(ii)Crystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 787306: Experimental Crystal Structure Determination

2011

Related Article: C.Bazzicalupi, A.Bencini, S.Ciattini, F.Denat, P.Desogere, C.Goze, I.Matera, B.Valtancoli|2010|Dalton Trans.|39|11643|doi:10.1039/c0dt00948b

Space GroupCrystallography17-(22'-(Diphenyl ether)dimethyl)-410-diazonia-17-diaza-cyclododecane tetrachloro-zinc(ii) monohydrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 787305: Experimental Crystal Structure Determination

2011

Related Article: C.Bazzicalupi, A.Bencini, S.Ciattini, F.Denat, P.Desogere, C.Goze, I.Matera, B.Valtancoli|2010|Dalton Trans.|39|11643|doi:10.1039/c0dt00948b

17-(22'-(Diphenyl ether)dimethyl)-410-diazonia-17-diaza-cyclododecane diperchlorateSpace GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

CCDC 787308: Experimental Crystal Structure Determination

2011

Related Article: C.Bazzicalupi, A.Bencini, S.Ciattini, F.Denat, P.Desogere, C.Goze, I.Matera, B.Valtancoli|2010|Dalton Trans.|39|11643|doi:10.1039/c0dt00948b

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters(17-(dibenzofuran-18-diyldimethyl)-14710-tetraza-cyclododecane)-copper(ii) bis(hexafluorophosphate) acetonitrile solvateExperimental 3D Coordinates

researchProduct

CCDC 787304: Experimental Crystal Structure Determination

2011

Related Article: C.Bazzicalupi, A.Bencini, S.Ciattini, F.Denat, P.Desogere, C.Goze, I.Matera, B.Valtancoli|2010|Dalton Trans.|39|11643|doi:10.1039/c0dt00948b

Space GroupCrystallographyCrystal System17-(Dibenzofuran-18-diyldimethyl)-4-azonia-1710-triaza-cyclododecane 17-(dibenzofuran-18-diyldimethyl)-14710-tetraza-cyclododecane perchlorate hydrateCrystal StructureCell ParametersExperimental 3D Coordinates

researchProduct

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