0000000001308271
AUTHOR
D. Zhukov
1H, 13C, 15N NMR, ESI mass spectral and single crystal X-ray structural characterization of three spiro[pyrrolidine-2,3′-oxindoles]
Abstract Three spiro[pyrrolidine-2,3′-oxindoles], 1,1′,2,2′,5′,6′,7′,7′a-octahydro-2-oxo-1′-phenyl-spiro[3H-indole-3,3′-[3H]-pyrrolizine]-2′-carboxylic acid methyl ester (1), 1,1′,2,2′,5′,6′,7′,7′a-octahydro-2-oxo-1′-nitro-2′-phenyl-spiro[3H-indole-3, 3′-[3H]-pyrrolizine] (2) and 1,1′,2,2′,5′,6′,7′,7′a-octahydro-2-oxo-1′-nitro-2′-(4″-chlorophenyl)-spiro[3H-indole-3,3′-[3H]-pyrrolizine] (3) have been synthesized and their 1H, 13C and 15N spectra assigned. The chemical shift assignments are based on Pulsed Field Gradient (PFG) Double Quantum Filter (DQF) 1H, 1H correlation spectroscopy (COSY), PFG 1H, 13C Heteronuclear Multiple Quantum Coherence (HMQC) and PFG 1H,X (X = 13C and 15N) Heteronuc…
CCDC 289303: Experimental Crystal Structure Determination
Related Article: K.Laihia, A.Valkonen, E.Kolehmainen, A.Antonov, D.Zhukov, I.Fedosov, V.Nikiforov|2006|J.Mol.Struct.|800|100|doi:10.1016/j.molstruc.2006.03.095
CCDC 289301: Experimental Crystal Structure Determination
Related Article: K.Laihia, A.Valkonen, E.Kolehmainen, A.Antonov, D.Zhukov, I.Fedosov, V.Nikiforov|2006|J.Mol.Struct.|800|100|doi:10.1016/j.molstruc.2006.03.095
CCDC 289302: Experimental Crystal Structure Determination
Related Article: K.Laihia, A.Valkonen, E.Kolehmainen, A.Antonov, D.Zhukov, I.Fedosov, V.Nikiforov|2006|J.Mol.Struct.|800|100|doi:10.1016/j.molstruc.2006.03.095