6533b7d0fe1ef96bd125b75f

RESEARCH PRODUCT

Procedures of Separation and Pre‐concentration for Molybdenum Determination Using Atomic Spectrometry—a Review

Antonio Celso Spinola CostaSergio Luis Costa FerreiraHilda C. Dos SantosMiguel De La Guardia

subject

ChromatographyChemistryExtraction (chemistry)Analytical chemistryAnalytical proceduresAtomic spectroscopyMicrowave digestionInductively coupled plasmaGraphite furnace atomic absorptionMass spectrometryInstrumentationInductively coupled plasma mass spectrometrySpectroscopy

description

Abstract The literature concerning the improvement of atomic and ionic procedures for molybdenum determination through separation and pre‐concentration were updated. Analytical procedures based on flame atomic absorption spectrometry (AAAS), electrothermal or graphite furnace atomic absorption spectrometry (GFAAS), inductively coupled plasma optical emission spectrometry (ICP‐OES), and inductively coupled plasma mass spectrometry were reviewed taking into consideration the preliminary steps, which can enhance the selectivity and sensitivity based on co‐precipitation, solvent extraction, and solid‐phase extraction. Both in‐batch and on‐line procedures were considered.

https://doi.org/10.1081/asr-120037147