6533b7d2fe1ef96bd125ea6b

RESEARCH PRODUCT

An EC-branch in the decay of 27-s 263Db: Evidence for the isotope 263Rf

B. SchaustenU. RiethP. A. WilkBernhard KuczewskiKenneth E. GregorichC. A. LaueHeino NitscheJ. V. KratzA. NählerA. KronenbergW. BrüchleHeinz W. GäggelerRalf SudoweErik StrubAndreas TürlerD.t. JostMatthias Schädel

subject

Chemical separationchemistry.chemical_compoundCyclohexanechemistryIsotopeElutionAnalytical chemistryHalf-lifeNuclidePhysical and Theoretical Chemistry

description

Summary 27-s 263Db was produced in the 249Bk ( 18O, 4n) reaction at 93 MeV. The activity was transported by a He/KCl-jet to the laboratory where it was collected for 15 min and then subjected to a chemical separation specific for group-4 elements. The activity was dissolved in 0.5 M unbuffered α-HiB and eluted from a cation-exchange column. The effluent was made 9 M in HCl and group-4 tetrachlorides were extracted into TBP/Cyclohexane which was evaporated to dryness on a Ta disc. The Ta discs were assayed for α and SF activity. A SF activity with a half life on the order of 20 min was observed and assigned to the nuclide 263Rf. It is formed by electron-capture decay of 263Db with a decay branch of 3+4 -1%.

https://doi.org/10.1524/ract.91.1.59.19010