A facile microsynthesis of 14C-labelled picene

6533b7d6fe1ef96bd12663d4

RESEARCH PRODUCT

A facile microsynthesis of 14C-labelled picene

Albrecht Seidel D. Beermann Franz Oesch Peter Petrovic

subject

Aryl Organic Chemistry Phosphonium salt Biochemistry Analytical Chemistry chemistry.chemical_compound Picene chemistry Yield (chemistry)Drug Discovery Wittig reaction Organic chemistry Radiology Nuclear Medicine and imaging Spectroscopy Microscale chemistry

description

Microscale Wittig olefination of commercially available [7-14C]-benzal dehyde of high specific radioactivity with aryl bromomethyl phosphonium salt and subsequent oxidative photocyclisation affords pure 14C-labelled picene in efficient yield.

year	journal	country	edition	language
1984-08-01	Journal of Labelled Compounds and Radiopharmaceuticals

https://doi.org/10.1002/jlcr.2580210812

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