6533b7dafe1ef96bd126f61e
RESEARCH PRODUCT
Multi‐Mycotoxin Analysis in Durum Wheat Pasta by Liquid Chromatography Coupled to Quadrupole Orbitrap Mass Spectrometry
Alberto RitieniEmilia FerrerJordi MañesGiulia GrazianiJosefa TolosaDonato ChianeseAnna Gasparisubject
Fumonisin B1AflatoxinChromatographyHealth Toxicology and Mutagenesis010401 analytical chemistrybaby‐food; durum wheat pasta; multi‐residual method; HRMS‐orbitrap04 agricultural and veterinary sciencesToxicologyOrbitrap040401 food science01 natural sciencesBeauvericin0104 chemical scienceslaw.inventionBaby foodchemistry.chemical_compound0404 agricultural biotechnologychemistrylawFood scienceMycotoxinZearalenoneFood contaminantdescription
A simple and rapid multi‐mycotoxin method for the determination of 17 mycotoxins simultaneously is described in the present survey on durum and soft wheat pasta samples. Mycotoxins included in the study were those mainly reported in cereal samples: ochratoxin‐A (OTA), aflatoxin B1 (AFB1), zearalenone (ZON), deoxynivalenol (DON), 3‐and 15‐acetyl‐deoxynivalenol (3‐AcDON and 15‐AcDON), nivalenol (NIV), neosolaniol (NEO), fusarenon‐X, (FUS‐X), T‐2 toxin (T‐2) and HT‐2 toxin (HT‐2), fumonisin B1 and B2 (FB1 and FB2), and four emerging mycotoxins: three enniatins (ENA, ENA1, and ENB), and beauvericin (BEA). Twenty‐nine samples were analyzed to provide an overview on mycotoxin presence: 27 samples of durum wheat pasta, and two samples of baby food. Analytical results concluded that trichothecenes showed the highest incidence, mainly DON, NIV, and HT‐2 toxin, followed by ZON and ENB, while NEO, FUS‐X, OTA, AFB1, and FUM were not detected in any sample. The highest contents corresponded to ENB and ranged from 91.15μg/kg to 710.90 μg/kg.
year | journal | country | edition | language |
---|---|---|---|---|
2017-02-09 | Toxins; Volume 9; Issue 2; Pages: 59 |