Holskābes metilestera solvātu iegūšana un desolvatācija Holskābes metilestera solvātu iegūšana un desolvatācija

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Holskābes metilestera solvātu iegūšana un desolvatācija Holskābes metilestera solvātu iegūšana un desolvatācija

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Holskābes metilestera solvātu iegūšana un desolvatācija. Zvaniņa D., darba vadītājs Mg.Chem. Bērziņš A. Bakalaura darbs, 56 lappuses, 28 attēli, 2 tabulas, 40 literatūras avoti, 3 pielikumi. Latviešu valodā. Darbā tika pagatavoti holskābes metilestera metanola, etanola, acetonitrila un nitrometāna solvāti, un ar dažādām metodēm tika mēģināts iegūt holskābes metilestera hidrātu. Ar pulvera rentgendifraktometru ir pārbaudīts vai iegūti vēlamie solvāti. Ar pulvera rentgendifraktometru, rentgendifraktometra termokameru un derivatogrāfu tika pētīts solvātu desolvatācijas mehānisms un karsēšanas laikā notiekošās fāžu pārejas. Ar derivatogrāfu tika analizēti holskābes metilestera metanola un etanola solvātu desolvatācijas kinētika. Abiem solvātiem tika rēķināta aktivācijas enerģija, noteikts desolvatācijas procesa kinētiskais modelis. HOLSKĀBES METILESTERIS, SOLVĀTI, DESOLVATĀCIJA, AKTIVĀCIJAS ENERĢIJA, PULVERA RENTGENDIFRAKTOMETRS, DIFERENCIĀLĀ TERMISKĀ ANALĪZE.

year	journal	country	edition	language
2013-01-01

https://dspace.lu.lv/dspace/handle/7/22899

PEPhysical Sciences and Engineering
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