Zur Chemie und Pharmakologie der Alkaloide Damascenin und Arecolin 1. Mitt.: Beiträge zur Synthese von Damascenin und Damasceninhomologen

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Zur Chemie und Pharmakologie der Alkaloide Damascenin und Arecolin 1. Mitt.: Beiträge zur Synthese von Damascenin und Damasceninhomologen

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Ausgehend von der 3-Methoxybenzoesaure wurde eine verbesserte Damasceninsynthese gefunden: 3-Methoxy-benzoesaure wird mit Methanol und HCl-Gas verestert, der Ester bei Temperaturen von etwa —10° in Acetanhydrid mit konzentrierter Salpetersaure nitriert und nach katalytischer Reduktion mit Raney-Nickel mit Methyljodid methyliert. In Anlehnung an die Damasceninsynthese von Kaufmann und Rothlin wurde der 3-Athoxy-2-athylamino-benzoesauremethylester hergestellt.

year	journal	country	edition	language
1965-01-01	Archiv der Pharmazie

https://doi.org/10.1002/ardp.19652981209

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