6533b820fe1ef96bd12798f3

RESEARCH PRODUCT

High-resolution transmission electron microscopic investigations of molybdenum thin films on faceted α-Al2O3

Michael HuthJ. OsterLeonore Wiehl

subject

FacetingOrientation (vector space)CrystallographyChemistryTransmission electron microscopyengineeringCorundumThin filmengineering.materialFacetEpitaxyHigh-resolution transmission electron microscopyGeneral Biochemistry Genetics and Molecular Biology

description

Epitaxially grown Mo films on a faceted corundum (α-Al2O3)mplane were investigated by transmission electron microscopy. Low- and high-resolution images were taken from a cross-section specimen cut perpendicular to the facets. It was possible to identify unambiguously the crystallographic orientation of these facets and explain the considerable deviation (∼10°) of the experimental interfacet angle, as measured with atomic force microscopy (AFM), from the expected value. For the first time, proof is given for a smooth \{10\bar{1}1\} facet and a curvy facet with orientation near to \{10\bar{1}\bar{2}\}. Moreover, the three-dimensional epitaxial relationship of an Mo film on a faceted corundummsurface was determined.

https://doi.org/10.1107/s0021889804033126