6533b824fe1ef96bd1280d04

RESEARCH PRODUCT

Microstructural evolution and growth of crystallite size of mullite during thermal transformation of kyanite

F. J. SerranoAngel CaballeroJoaquín BastidaM.a. Sainz

subject

Platelet MorphologyMicrostructural evolutionMaterials scienceThermal transformationMineralogyMulliteAtmospheric temperature rangeKyanitevisual_artMaterials ChemistryCeramics and Compositesvisual_art.visual_art_mediumCrystalliteComposite material

description

Abstract The microstructural evolution of mullite during the thermal transformation of kyanite has been studied in the temperature range 1200–1600 °C. The shape and size of the grains were analysed by means of SEM-EDS while crystallite size evolution was studied by X-ray line profile analyses. The results obtained showed that total transformation of kyanite to mullite takes place between 1350 and 1400 °C. At temperatures below 1350 °C needle-like mullite grains are always produced. At higher temperatures the mullite grains reveal rounded end platelet morphology. Evolution from needle-like to platelet shape was correlated with the X-ray data.

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