ChemInform Abstract: Synthesis of Areno-Condensed [24]Annulenes.

6533b825fe1ef96bd1282651

RESEARCH PRODUCT

ChemInform Abstract: Synthesis of Areno-Condensed [24]Annulenes.

Herbert Meier Michael Fetten Christoph Schnorpfeil

subject

Chrysene chemistry.chemical_compound Crystallography Differential scanning calorimetry chemistry Alkoxy group Molecule General Medicine Annulene Solubility Condensation reaction Ring (chemistry)

description

[24]Annulenes condensed with three phenanthrene units (11a−d) or with three chrysene ring systems (22) were prepared by multi-step syntheses. The cyclic condensation reaction in the final step led to highly symmetrical compounds. Long flexible alkoxy groups attached to the periphery enhance the solubility and give rise to a strong aggregation of the molecules which was observed in solution by NMR and fluorescence excitation spectroscopy, and in the pure state by the detection of liquid crystalline phases in differential scanning calorimetry and polarization microscopy.

year	journal	country	edition	language
2010-05-23	ChemInform

https://doi.org/10.1002/chin.200204133

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