Étude par microscopie électronique et spectroscopie de films minces catalytiques pour micro piles à combustibles

6533b827fe1ef96bd12861c6

RESEARCH PRODUCT

Étude par microscopie électronique et spectroscopie de films minces catalytiques pour micro piles à combustibles

Jaroslava Lavková

subject

Palivové články Fuel cell Transmisní elektronový mikroskop Cer oxid Cerium oxide Pulvérisation cathodique magnétron [CHIM.THEO] Chemical Sciences/Theoretical and/or physical chemistry Magnetronové naprašování Oxyde de cérium Platine Pile à combustible Platina Transmission Electron Microscopy Microscopie électronique en transmission Magnetron sputtering Platinum

description

Předložená dizertační práce se zabývá studiem nových katalyzátorů na bázi kov-oxid vhodných pro použití v palivových článcích na straně anody. Platinou dopovaný oxid ceru připravený magnetronovým naprašováním ve formě tenkých vrstev na uhlíkových mezivrstvách nesených křemíkovým substrátem byl zkoumán prostřednictvím mikroskopických a spektroskopických metod. Vliv složení uhlíkového nosiče (a-C a CNx filmy), depozičního času CeOx vrstvy a dalších depozičních parametrů, např. depoziční rychlosti, složení pracovní atmosféry a Pt koncentrace na morfologii Pt-CeOx vrstev byl studován převážně pomocí transmisní elektronové mikroskopie (TEM). Získané výsledky ukazují, že vhodnou kombinací depozičních podmínek jsme schopni vyladit výslednou morfologii a kompozici katalyzátoru. Složení uhlíkových filmů a Pt-CeOx vrstev bylo studováno spektroskopickými technikami – energiově-disperzní spektroskopií (EDX), spektroskopií charakteristických ztrát elektronů (EELS) a rentgenovou fotoelektronovou spektroskopií (XPS). Takto připravené porézní struktury vrstev Pt-CeOx jsou slibným katalytickým materiálem na straně anody pro reálné aplikace v palivových článcích.

year	journal	country	edition	language
2016-01-01

https://theses.hal.science/tel-01697223

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