6533b831fe1ef96bd1298e11
RESEARCH PRODUCT
Investigation of TiO<sub>2</sub> Ceramic Surface Conductivity Using Conductive Atomic Force Microscopy
Jurijs OzolinsK. KundzinsJanis LocsKristaps Rubenissubject
AnataseMaterials scienceScanning electron microscopeMechanical EngineeringAnalytical chemistryConductive atomic force microscopyConductivitySurface conductivityMechanics of Materialsvisual_artvisual_art.visual_art_mediumGeneral Materials ScienceGrain boundaryCeramicPhotoconductive atomic force microscopydescription
Dense TiO2 (rutile) ceramic samples were prepared by sintering compacts of titanium dioxide anatase powder at 1500 °C for 5h. Sintered samples were polished and annealed in vacuum at 1000 °C for 1h. Structural properties of the samples were studied by X-ray diffraction, polarized light and scanning electron microscopy. The surface topography and local electrical conductivity of the samples were investigated by atomic force microscopy technique under atmospheric conditions. Enhanced electrical conductivity was observed at grain boundaries while the polished, vacuum annealed grains surface showed non-homogeneous conductivity.
year | journal | country | edition | language |
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2012-11-01 | Key Engineering Materials |