Regioisomeric 5(3)-aminomethyl-3(5)-phenylisoxazoles: synthesis, spectroscopic discrimination, and muscarinic activity.

6533b836fe1ef96bd12a0a28

RESEARCH PRODUCT

Regioisomeric 5(3)-aminomethyl-3(5)-phenylisoxazoles: synthesis, spectroscopic discrimination, and muscarinic activity.

Günter Lambrecht Ernst Mutschler Stefan Laufer J. Schweiger Gerd Dannhardt

subject

Male Tertiary amine Stereochemistry Chemistry Guinea Pigs Vas deferens Cholinergic Agents Pharmaceutical Science Muscle Smooth In Vitro Techniques Chemical synthesis Mass spectrometric Myocardial Contraction medicine.anatomical_structure Vas Deferens Ileum Drug Discovery Muscarinic acetylcholine receptor Structural isomer medicine Animals Rabbits Oxazoles Muscle Contraction

description

The regioselective synthesis of isomeric 5(3)-aminomethyl-3(5)-phenyl isoxazoles using different methods is described. Spectroscopic data, especially mass spectrometric fragmentation, were used to identify and characterize the regioisomers. The muscarinic activity of these isoxazoles was assayed on isolated guinea-pig ileum and atria as well as on isolated rabbit vas deferens. Regioisomere 5(3)-Aminomethyl-3(5)-phenyl-isoxazole: Synthese, spektroskopische Unterscheidung und muskarinische Aktivitat Es werden verschiedene Verfahren zur regioselektiven Darstellung von 5(3)-Aminomethyl-3(5)-phenyl-isoxazolen beschrieben, die anhand ihrer spektroskopischen Daten, insbesondere der massenspektroskopischen Fragmentierung, zuverlassig unterschieden werden konnen. Am isolierten Meerschweinchenileum bzw.-atrium sowie am isolierten Vas deferens des Kaninchens wird die muskarinische Aktivitat der phenylsubstituierten Aminomethylisoxazole gepruft.

year	journal	country	edition	language
1995-05-01	Archiv der Pharmazie

10.1002/ardp.19953280508 https://pubmed.ncbi.nlm.nih.gov/7611839

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