6533b836fe1ef96bd12a1b72

RESEARCH PRODUCT

Gas-chromatographic elemental analysis via di(trifluorethyl)dithiocarbamato-chelates

H. SchallerRolf Neeb

subject

Detection limitAqueous solutionChromatographyChemistryClinical BiochemistryExtraction (chemistry)General MedicineAnalytical ChemistryMetalElemental analysisvisual_artvisual_art.visual_art_mediumPh rangeGeneral Materials ScienceChelationTrace metal

description

The capillary-gas-chromatographic conditions for the determination of trace metals after extraction from aqueous solution are optimized by coupling of capillaries and improvement of injection technique. Different detectors (FID and ECD) are tested. pH range and buffer systems for extraction of metal chelates are discussed.

https://doi.org/10.1007/bf00470763