6533b854fe1ef96bd12ae84c
RESEARCH PRODUCT
Adsorptionsvoltammetrische Molybd�nbestimmung in biologischen Proben nach nassem Hochdruckaufschlu\
Elisabeth CziollekRolf Neebsubject
ChromatographyChemistryClinical BiochemistryAnalytical chemistryGeneral MedicineBiochemistryDecompositionBiological materialsAnalytical ChemistryMatrix (chemical analysis)High pressureGeneral Materials ScienceSeawaterSpecial caredescription
The transfer of an (known from literature [141 and till now only applied to seawater) adsorption-voltammetric determination of molybdenum with oxine to biological samples, is described. The herewith accomplished changes of base solution resulted simultaneously in an optimization of the method with regard to interpretability and sensitivity. Special care was taken in the problem of decomposition. Best results are obtained with a high-pressure decomposition. Accuracy of analyses is confirmed with trials of recovery also in the biological matrix.
| year | journal | country | edition | language |
|---|---|---|---|---|
| 1989-12-01 | Fresenius' Zeitschrift f�r Analytische Chemie |