Effect of Polymer Length on the Adsorption onto Aluminogermanate Imogolite Nanotubes

6533b857fe1ef96bd12b502c

RESEARCH PRODUCT

Effect of Polymer Length on the Adsorption onto Aluminogermanate Imogolite Nanotubes

Giuseppe Cavallaro Frédéric Pignon Erwan Paineau Giuseppe Lazzara Leonardo Chiappisi

subject

Nanotube Materials science Imogolite 02 engineering and technology Calorimetry Neutron scattering 010402 general chemistry 01 natural sciences Settore CHIM/12 - Chimica Dell'Ambiente E Dei Beni Culturali chemistry.chemical_compound Adsorption Rheology Electrochemistry General Materials Science ComputingMilieux_MISCELLANEOUS Spectroscopy Settore CHIM/02 - Chimica Fisica chemistry.chemical_classification Quantitative Biology::Biomolecules Surfaces and Interfaces Polymer Polyethylene 021001 nanoscience & nanotechnology Condensed Matter Physics 0104 chemical sciences Condensed Matter::Soft Condensed Matter chemistry Chemical engineering Imogolite nanotubes SANS ITC PEGs [PHYS.PHYS.PHYS-CHEM-PH]Physics [physics]/Physics [physics]/Chemical Physics [physics.chem-ph]0210 nano-technology [PHYS.COND.CM-SCM]Physics [physics]/Condensed Matter [cond-mat]/Soft Condensed Matter [cond-mat.soft]

description

This study evidences the adsorption of model nonionic polymers onto aluminogermanate imogolite nanotubes, attractive porous nanofillers with potential molecular loading and release applications. We resolve the underlying mechanisms between nanotubes and polyethylene glycols with different molecular weights by means of nanoisothermal titration calorimetry. The analysis of the results provides a direct thermodynamic characterization, allowing us to propose a detailed description of the energetics involved in the formation of polymer/imogolite complexes. The affinity toward the nanotube surface is enthalpy-driven and strongly depends on the polymer chain length, which significantly affects the polymer configuration and the flow properties of the resulting complexes, probed by small-angle neutron scattering and rheology, respectively. These findings open new avenues for the rational design of these hybrid mixtures for advanced applications.

year	journal	country	edition	language
2021-08-17

10.1021/acs.langmuir.1c01549 http://hdl.handle.net/10447/539019

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