Paraugu sagatavošanas metodes optimizācija farmaceitisko savienojumu noteikšanai notekūdens paraugos

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RESEARCH PRODUCT

Paraugu sagatavošanas metodes optimizācija farmaceitisko savienojumu noteikšanai notekūdens paraugos

Veronika ŠUkajeva

subject

DIVDIMENSIJU ŠĶIDRUMA HROMATOGRĀFIJA - MASAS SPEKTROMETRIJA CIETFĀZES ESKTRAKCIJA EPIDEMIOLOĢIJA FARMACEITISKIE SAVIENOJUMI ANALĪTISKĀS METODES OPTIMIZĀCIJA Ķīmija

description

Paraugu sagatavošanas metodes optimizācija farmaceitisko savienojumu noteikšanai notekūdens paraugos. Šukajeva V., zinātniskā vadītāja Mag. ķīm. Ikkere L.E. Bakalaura darbs, 59 lpp., 11 attēli, 16 tabulas, 37 literatūras avoti, 1 pielikums. Latviešu valodā. Bakalaura darba ietvaros tika veikta literatūras avotu izpēte par uz notekūdeņiem balstītu epidemioloģiju, Latvijā izplātītākiem farmaceitiski aktīviem savienojumiem, populācijas biomarķieriem un farmaceitisko savienojumu noteikšanas tendencēm ūdens matricās. Klasiskā SPE metode tika optimizēta 56 farmaceitiski aktīvo savienojumu noteikšanai notekūdens paraugos. SPE metodes optimizēšanai tika salīdzinātās Oasis® HLB un dažādas Strata™ kolonnas, kā arī dažādi procedūras apstākļi. Papildus tika izstrādāta atšķaidīšanas metode 6 pārējiem farmaceitiski aktīviem savienojumiem un populācijas biomarķieriem. SPE un atšķaidīšanas metožu validācija tika veikta, izmantojot 2D-LC-MS instrumentālo analīzi. Optimizētās metodes tika pielietotas 28 notekūdens paraugu analīzei, kuros tika konstatēti 44 no 62 analizējamiem savienojumiem.

year	journal	country	edition	language
2021-01-01

https://dspace.lu.lv/dspace/handle/7/55140

PEPhysical Sciences and Engineering
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