6533b85bfe1ef96bd12bbe47
RESEARCH PRODUCT
ChemInform Abstract: Solution Synthesis of a New Thermoelectric Zn1+xSb Nanophase and Its Structure Determination Using Automated Electron Diffraction Tomography.
Christina S. BirkelEnrico MugnaioliWolfgang TremelTatiana GorelikMartin PanthoeferUte Kolbsubject
Chemical engineeringElectron diffractionChemistryThermoelectric effectNanoparticleGeneral MedicineSolution synthesisTomographydescription
Thermoelectric nanoparticles of the nominal composition Zn4Sb3 are prepared by heating Sb nanoparticles with a 9-fold excess of Zn particles (synthesized by reaction of SbCl3 or ZnCl2 with Li[Et3BH] in THF at room temperature, and about 65 °C, respectively) in trioctylamine at about 300 °C for 225 min.
| year | journal | country | edition | language |
|---|---|---|---|---|
| 2010-09-30 | ChemInform |