Titanium Complexes with a Linked Amido−Cyclopentadienyl Ligand and a Bidentate Organyl Group: Synthesis, Structure, and Ethene Polymerization Activity

6533b86efe1ef96bd12cb613

RESEARCH PRODUCT

Titanium Complexes with a Linked Amido−Cyclopentadienyl Ligand and a Bidentate Organyl Group: Synthesis, Structure, and Ethene Polymerization Activity

Thomas Eberle Thomas P. Spaniol Jun Okuda

subject

Denticity Chemistry Ligand Methylaluminoxane chemistry.chemical_element Photochemistry Medicinal chemistry Square pyramidal molecular geometry Inorganic Chemistry chemistry.chemical_compound Polymerization Cyclopentadienyl complex Isopropyl Titanium

description

Titanium complexes containing a linked isopropyl- or benzylamido(tetramethylcyclopentadienyl) ligand C5Me4SiMe2NR (R = iPr, CH2Ph,) and one bidentate organyl group C6H4(CH2NMe2)-2, CH2C6H4(NMe2)-2, and {η5-C5H3(CH2NMe2)-2}Fe(η5-C5H5) were prepared by salt metathesis of the corresponding dichloro complex Ti(η5:η1-C5Me4SiMe2NR)Cl2 with the lithium organyl. Single crystal X-ray structural analysis of Ti(η5:η1-C5Me4SiMe2NCH2Ph)- {C6H4(CH2NMe2)-2}Cl and of Ti(η5:η1-C5Me4SiMe2NiPr){CH2C6H4(NMe2)-2}Cl revealed the presence of intramolecular coordination with square pyramidal geometry around titanium. In the ferrocenyl derivative Ti(η5:η1-C5Me4SiMe2NCH2Ph)[{η5-C5H3(CH2NMe2)-2}Fe(η5-C5H5)]Cl the NMe2 group is not bonded at the titanium atom. Ethene polymerization catalyzed by these complexes upon activation with methylaluminoxane was examined.

year	journal	country	edition	language
1998-02-01	European Journal of Inorganic Chemistry

https://doi.org/10.1002/(sici)1099-0682(199802)1998:2<237::aid-ejic237>3.0.co;2-p

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