ICP-MS multielement determination in fly ash after microwave-assisted digestion of samples.

6533b870fe1ef96bd12cfc9c

RESEARCH PRODUCT

ICP-MS multielement determination in fly ash after microwave-assisted digestion of samples.

Arabinda K. Das M. Luisa Cervera Debasis Goswami Miguel De La Guardia Ruma Chakraborty

subject

Chromatography Microwave assisted digestion Digestion (alchemy)Chemistry Fly ash Microwave oven Neutron activation analysis Mass spectrometry Inductively coupled plasma mass spectrometry Dissolution Analytical Chemistry

description

A microwave assisted digestion procedure has been developed for dissolution of fly ash samples prior to the inductively coupled plasma-mass spectrometric determination of their elemental composition. The developed methodology was validated by carrying out the analysis of two high-silicate containing reference materials (CRM 134R sewage amended soil and NIES JR 1 rock) and by means of the comparison between results found by microwave-assisted digestion and ICP-MS of fly ash samples with those found by neutron activation analysis (NAA) for Sb, Cs, Cr, Co, Fe, U and Zn determination. The method developed can be recommended for routine multielement analysis of fly ash.

year	journal	country	edition	language
2001-06-21	Talanta

10.1016/s0039-9140(01)00370-8 https://pubmed.ncbi.nlm.nih.gov/18968321

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