Search results for " Analytic"

Investigation on four centuripe vases (late 3rd-2nd cent. B.C.) by portable X-ray fluorescence and total reflectance-FTIR

2021

Abstract Four Centuripe vases dated back to the late 3rd-2nd centuries B.C. were analysed using imaging under visible and ultra-violet illumination as well as complementary non-invasive and non-destructive portable X-Ray Fluorescence (XRF) and Total Reflectance – Fourier Transform InfraRed (TR-FTIR) spectroscopies. The vases are of great importance since they represent a rare expression of the Hellenistic vase painting. Four specimens, a “pyxis”, a “lebes gamikos” and two “lekanides” decorated with figures of different type, are exhibited in the Antonino Salinas Archaeological Museum in Palermo-Italy. The investigation was aimed to identify the used pigments and the painting technique, to r…

Non-Invasive Investigation of Pigments of Wall Painting in S. Maria Delle Palate di Tusa (Messina, Italy)

2019

The characterization of materials used in the archaeological field needs an experimental approach in order to avoid the destruction or perturbation of artworks. In order to afford this purpose, a multi-analytical spectroscopic approach is regularly used. We combined non-invasive analysis by using handheld spectroscopic instrumentations (mainly XRF and Raman spectrometers) in order to characterize the wall painting preserved in the church of S. Maria delle Palate at Halaesa Arconidea archeological site (Tusa, Messina, Italy). The aim of the work is the characterization of the nature of pigments used for the realization of the wall painting. The wall painting, probably representing St. Franci…

New insights to assess the consolidation of stone materials used in built heritage: the case study of ancient graffiti (Tituli Picti) in the archaeol…

2020

AbstractTituli Picti are an ancient form of urban graffiti very common in the archaeological site of Pompeii (Naples, South—Italy). They are generally made of red pigments applied on walls of Campanian ignimbrite. This paper deals with a scientific investigation aimed to their conservation. This is a challenging task since it requires a multidisciplinary approach that includes restorers, archaeologists and conservation scientists. The study has provided suggestions on the proper way to conserve Tituli Picti over time. In the present work, several specimens of Campanian ignimbrite were painted with red earth pigment; lime and Arabic gum have been used as binders as well. Such painted stones …

Digitization and Preservation of Cultural Heritage Products

2017

Cultural heritage encompasses various aspects of a nation's history. Cultural heritage artifacts are considered as priceless items that need special care. Since the wide adoption of new digital technologies, documenting and storing cultural heritage assets became more affordable and reliable. These records are then used in several applications. Researchers saw the opportunity to use digital heritage recordings for long-term preservation. They are considering cultural heritage artifacts as products, and the history behind them as a product lifecycle. In this paper, we present the research progress in cultural heritage digital processing and preservation, highlighting the most impactful advan…

Study of the performance of a resolution criterion to characterise complex chromatograms with unknowns or without standards

2017

The search for best conditions in liquid chromatography is routinely carried out with information provided by chemical standards. However, sometimes there are samples with insufficient knowledge about their chemical composition. In other cases, identities of the components are known, but there are no standards available, and in other cases the identities of peaks in chromatograms taken under different conditions are ambiguous. Most resolution criteria used to measure separation performance cannot be applied to these samples. In this work, a global resolution function valid for all situations was developed based on automatic measurements of peak prominences (area fraction exceeding the line …

Commentaria Ioannis Grammatici Alexandrei cognomento Philoponi in libros posteriorum Aristotelis

Sig. A-N6, O8 Els grav. xil. son figures geomètriques. - Capitals grav., frisos, etc Text a dos col., amb postil·les marginals. - Reclams. - Registre

Midinfrared FT-IR as a Tool for Monitoring Herbaceous Biomass Composition and Its Conversion to Furfural

2015

A semiquantitative analysis by means of midinfrared FT-IR spectroscopy was tuned for the simultaneous determination of cellulose, hemicellulose, and lignin in industrial crops such as giant reed (Arundo donaxL.) and switchgrass (Panicum virgatumL.). Ternary mixtures of pure cellulose, hemicellulose, and lignin were prepared and a direct correlation area/concentration was achieved for cellulose and lignin, whereas indirect correlations were found for hemicellulose quantification. Good correspondences between the values derived from our model and those reported in the literature or obtained according to the official Van Soest method were ascertained. Average contents of 40–45% of cellulose, 2…

Wireless Acoustic Sensor Networks and Applications

2017

Hair Mercury Levels Detection in Fishermen from Sicily (Italy) by ICP-MS Method after Microwave-Assisted Digestion

2015

A number of ninety-six hair samples from Sicilian fishermen were examined for total mercury detection by an Inductively Coupled Plasma Mass Spectrometry (ICP-MS) method. The mercury levels obtained were compared with mercury levels of 96 hair samples from a control group, in order to assess potential exposure to heavy metals of Sicilian fishermen due to fish consumption and closeness to industrial activities. Furthermore, the mercury levels obtained from hair samples were sorted by sampling area in order to verify the possible risks linked to the different locations. The overall mean concentration in the hair of the population of fishermen was6.45±7.03 μg g−1, with a highest value in a fish…

Artificial Intelligence for Cybersecurity: A Systematic Mapping of Literature

2020

Due to the ever-increasing complexities in cybercrimes, there is the need for cybersecurity methods to be more robust and intelligent. This will make defense mechanisms to be capable of making real-time decisions that can effectively respond to sophisticated attacks. To support this, both researchers and practitioners need to be familiar with current methods of ensuring cybersecurity (CyberSec). In particular, the use of artificial intelligence for combating cybercrimes. However, there is lack of summaries on artificial intelligent methods for combating cybercrimes. To address this knowledge gap, this study sampled 131 articles from two main scholarly databases (ACM digital library and IEEE…