Search results for " Assisted"
showing 10 items of 241 documents
Microwave-Assisted Synthesis of New Selenazole Derivatives with Antiproliferative Activity
2013
New aryl-hydrazinyl-1,3-selenazole and aroyl-hydrazonyl-1,3-selenazoles were synthesized via Hantzsch type condensation reactions of selenosemicarbazides with α-halogenocarbonyl derivatives, under classical versus microwave heating conditions. Excellent yields and shorter reaction times were obtained under irradiation conditions. The structures of the synthesized compounds were assigned based on spectroscopic data (FT-IR, 1 H-NMR), MS and elemental analysis. Selenazole derivatives were screened for their anti-proliferative effects against two leukemia cell lines (CCRF-CEM and HL60) and three carcinoma cell lines (MDA-MB231, HCT116 and U87MG).
A photovoltaic charging system of an electrically assisted tricycle for touristic purposes
2013
In this paper the design, realization and testing of a photovoltaic charging system suitable for the management of an electrically power assisted tricycle are described. This vehicle uses a photovoltaic module as a source of electric energy for the battery recharging. In this work, an overview on the needs of sustainable mobility and on the commercial electrically power assisted velocipedes is presented. The electrical rickshaw prototype, developed in the SDELab laboratory of the University of Palermo, is presented in detail, underlining the design, implementation and developing phases of the photovoltaic charging system assembled on the velocipede. Moreover, tests oriented on the setting u…
Brevi note comparatistiche in tema di suicidio assistito
2019
The essay focuses on the legitimacy of assisted suicide in Italy and in England and Wales, particularly with regard to patients suffering from severe pain from incurable or terminal illnesses. In two recent cases (Cappato and Nicklinson), both Italian and English judges suggested to the Parliament to modify the current state of the law, without making a declaration of incompatibility with Article 8 of the Convention. The paper compares the approach of Corte Costituzionale and UK Supreme Court to the issue, revealing the ambiguity hidden behind those common decisions.
Dissimilarity Application for Medical Imaging Classification
2005
In the traditional way of learning from examples of objects the classifiers are built in a feature space. However, alternative ways can be found by constructing decision rules on dissimilarity (distance) representations. In such a recognition process a new object is described by its distances to (a subset of) die training samples. The use of the dissimilarities is especially of interest when features are difficult to obtain or when they have a little discriminative power. Purpose of this work is the development of an automatic classification system which could be useful for radiologists in the investigation of breast cancer. The software has been designed in the framework of the MAGIC-5 col…
Wider implications of video-assisted thoracic surgery versus open approach for lung metastasectomy
2015
ABSTRACT Lung metastasectomy is considered a safe and potentially curative procedure despite there is not a strong evidence that metastasectomy prolongs long-term survival in patients with lung metastases. Moreover, the debate is open regarding the best approach for lung metastasectomy, video-assisted thoracic surgery versus open approach. A systematic review of literature to clarify what is the best approach to prolong survival in patients with lung metastases was performed. Our study confirms that overall survival is equivalent for video-assisted thoracic surgery and thoracotomy, therefore the ‘gold standard’ surgical treatment for lung metastases remains a point of debate. The choice o…
Electrosynthesis of Ce–Co Mixed Oxide Nanotubes with High Aspect Ratio and Tunable Composition
2008
Cerium oxide and cobalt oxides have attracted the interest of several researchers due to their potential application in several technological fields electrochromism, lithium batteries, catalysis, etc.. Ceria has been used as a promoter in the so-called “three-way catalyst” for the control of toxic emission from automobile exhaust. The promotion consists of the enhancement of the noble metal dispersion, as well as stabilization of the supporting medium toward thermal sintering. 1,2 A direct catalytic effect of CeO2 in chemical processes such as water–gas shift reaction or NOx decomposition has been also evidenced. 3,4
ChemInform Abstract: Microwave-Assisted Organocatalytic Enantioselective Intramolecular Aza-Michael Reaction with α,β-Unsaturated Ketones.
2012
The combination of an epi-hydroquinine catalyst and pentafluoropropionic acid accelerates the process.
Ultrasound-assisted green solvent extraction of high-added value compounds from microalgae Nannochloropsis spp.
2015
Abstract The aim of this work was to investigate ultrasound (US)-assisted green solvent extraction of valuable compounds from the microalgae Nannochloropsis spp. Individual green solvents (water, ethanol (EtOH), dimethyl sulfoxide (DMSO)) and binary mixture of solvents (water-DMSO and water-EtOH) were used for the extraction procedures. Maximum total phenolic compounds yield ( Y p ≈ 0.33) was obtained after US pre-treatment ( W = 400 W, 15 min), being almost 5-folds higher compared to that found for the untreated samples and aqueous extraction ( Y p ≈ 0.06). The highest yield of total chlorophylls ( Y c ≈ 0.043) was obtained after US ( W = 400 W, 7.5 min), being more than 9-folds highe…
Interference-Based Chromatic Coatings by Ion Plating Plasma Assisted Deposition Technology
2010
The goal of replacing widespread and inexpensive galvanic treatments with suitable vacuum deposition techniques, in order to eliminate the environmental hazards and their polluting effects, is becoming, in some cases, more tangible. Shorter cleaning cycles, shorter pump-down times, reduced heating times of substrates and higher deposition rates allow the costs of new plasma-assisted processes to become competitive with respect to galvanic ones. Moreover, vacuum treatments offer superior mechanical and optical properties and non-conductive substrates (like glass, ceramics, plastics) can be more easily coated. This work describes the results obtained with Ion Plating Plasma Assisted depositio…
Focused microwave-assisted Soxhlet extraction: An expeditive approach for the isolation of lipids from sausage products
2003
A prototype of extractor based on the conventional Soxhlet principles but assisted in the cartridge zone by focused microwaves is proposed for accelerating the extraction of lipids from sausage products. The extraction process has been optimised using a multivariate design involving the main variables influencing the performance of the prototype (namely, irradiation power P, irradiation time T and number of cycles C). Under the optimum working conditions (P=160 W, T=10 s and C=14), the extraction of lipids from different Spanish sausage products is complete in 45 min. The extracts thus obtained have been compared with those provided by conventional Soxhlet extraction for 8 h by development …