Search results for " bonding"

showing 10 items of 934 documents

Crystal structure of chlorido-{4,5-dimeth-oxy-2-[(2,3-η)-2-prop-2-en-1-yl]phenyl-κC (1)}(piperidine-κN)platinum(II) ethanol monosolvate

2014

The title platinum(II) complex shows a trigonal–bipyramidal coordination and inter­molecular C—H⋯Cl, C—H⋯π and (C/O)—H⋯O hydrogen bonds.

crystal structureEthanolChemistryHydrogen bondchemistry.chemical_elementGeneral ChemistryCrystal structuremethyl­eugenolCondensed Matter Physicshydrogen bondingMedicinal chemistryResearch CommunicationsCrystallcsh:Chemistrychemistry.chemical_compoundmethyleugenollcsh:QD1-999General Materials SciencePiperidinePlatinumplatinum(II) complex
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A Simple Complex on the Verge of Breakdown: Isolation of the Elusive Cyanoformate Ion

2014

Cyanide Hitches a Ride Cyanide is a by-product of the biosynthesis of ethylene in plants and it has been somewhat puzzling how the ion is safely removed before it can shut down enzymatic pathways by coordination to catalytic iron centers. A proposed mechanism has implicated the cyanoformate ion—essentially, a weak adduct of cyanide and carbon dioxide—as the initial product, although its lifetime was uncertain. Murphy et al. (p. 75 ; see the Perspective by Alabugin and Mohamed ) crystallized this previously elusive adduct and found that its solution-phase stability varies inversely with the dielectric properties of the medium. The results bolster a picture in which the adduct shuttles the cy…

crystal structureEthyleneMagnetic Resonance SpectroscopyFormateskemiallinen sitoutuminenCyanideMineralogykiderakenneMedicinal chemistryIonCatalysisAdductchemistry.chemical_compoundsyanoformaattiX-Ray DiffractionCatalytic DomainNitrilesta116MultidisciplinaryAqueous solutionCyanidesMolecular StructureChemistrychemical bondingCarbon DioxideEthylenesThermodynamicsAmino Acid OxidoreductasescyanofrmateCrystallizationShut downScience
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N,N′-Bis(pyridin-2-yl)octanediamide

2016

The complete molecule of the title compound, C18H22N4O2, is generated by crystallographic inversion symmetry. In the crystal, N—H...N hydrogen bonds connect the molecules into [010] chains, which featureR22(8) loops. The packing is consolidated by C—H...O interactions.

crystal structureHydrogen bondAdamantaneadamantaneGeneral MedicineCrystal structure010402 general chemistry010403 inorganic & nuclear chemistryhydrogen bonding01 natural sciences0104 chemical sciencesCrystalCrystallographychemistry.chemical_compoundchemistryanti­viral effectslcsh:QD901-999lcsh:CrystallographyMOF self-assemblyantiviral effectsIUCrData
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Crystal structure and Hirshfeld surface analysis of (E)-1-[2,2-dichloro-1-(4-nitrophenyl)ethenyl]-2-(4-fluorophenyl)diazene

2019

The dihedral angle between the 4-fluoro­phenyl ring and the nitro-substituted benzene ring of the title compound is 63.29 (8)°. In the crystal, mol­ecules are linked by C—H⋯O hydrogen bonds into chains parallel to the c axis. The crystal packing is further stabilized by C—Cl⋯π, C—F⋯π and N—O⋯π inter­actions

crystal structureHydrogen bondChemistryStackingGeneral ChemistryCrystal structureDihedral angleCondensed Matter::Mesoscopic Systems and Quantum Hall EffectCondensed Matter PhysicsRing (chemistry)hydrogen bondingResearch Communications4-fluoro­phenyl ringCrystallcsh:ChemistryCrystallographylcsh:QD1-999Nitro4-fluorophenyl ringHirshfeld surface analysisGeneral Materials Sciencenitro-substituted benzene ringActa Crystallographica Section E: Crystallographic Communications
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Crystal structure of 4-(4-chlorophenyl)-6-(morpholin-4-yl)pyridazin-3(2H)-one

2015

In the crystal, pairs of centrosymmetrically related mol­ecules are linked into dimers via N—H⋯O hydrogen bonds, forming (8) ring motifs. The dimers are connected via C—H⋯O and C—H⋯Cl hydrogen bonds, forming a three-dimensional network·Semi-empirical mol­ecular orbital calculations were carried out using the AM1 method.

crystal structureHydrogen bondCyclohexane conformationStackingpi-pi stacking interactionsGeneral ChemistryCrystal structureDihedral anglehydrogen bondingCondensed Matter PhysicsRing (chemistry)Research Communicationslcsh:ChemistryCrystalchemistry.chemical_compoundCrystallographylcsh:QD1-999chemistryπ–π stacking interactionsMorpholineGeneral Materials Sciencepyridazinone derivativeπ–π stacking inter­actions
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Crystal structure of (E)-N-(3,4-di­meth­oxy­benzyl­idene)morpholin-4-amine

2014

In the title compound, C13H18N2O3, the benzene ring makes a dihedral angle of 17.19 (11)° with the least-squares plane formed by the four C atoms of the morpholine ring, which adopts a chair conformation. In the crystal, C—H...N hydrogen bonds link the molecules into supramolecular chains running along a 21screw axis parallel to theb-axis direction. Weak C—H...π interactions are also observed.

crystal structureHydrogen bondCyclohexane conformationSupramolecular chemistryGeneral ChemistryCrystal structureDihedral angleCondensed Matter PhysicsBioinformaticsRing (chemistry)hydrogen bondingC—H⋯π inter­actionsData Reportslcsh:ChemistryCrystalCrystallographychemistry.chemical_compoundC—H...π interactionslcsh:QD1-999chemistryMorpholineGeneral Materials ScienceSchiff basesC - H?? interactionsmorpholin-4-amineActa Crystallographica Section E: Structure Reports Online
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Crystal structure and Hirshfeld surface analysis of 2-[(1,3-benzoxazol-2-yl)sulfanyl]-N-(2-methoxyphenyl)acetamide

2019

Akkurt, Mehmet/0000-0003-2421-0929; Saylam, Merve/0000-0002-7602-4565

crystal structureHydrogen bondGeneral ChemistryCrystal structureDihedral angleCondensed Matter::Mesoscopic Systems and Quantum Hall Effecthydrogen bonding010402 general chemistry010403 inorganic & nuclear chemistryCondensed Matter PhysicsRing (chemistry)01 natural sciences13-benzoxazole ring system0104 chemical scienceslcsh:ChemistryCrystaldimerschemistry.chemical_compoundCrystallographylcsh:QD1-999chemistryHirshfeld surface analysisGeneral Materials ScienceBenzeneAcetamideActa Crystallographica Section E Crystallographic Communications
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Crystal structure of dimethylammonium hydrogen oxalate hemi(oxalic acid)

2015

The title salt consists of a di­methyl­ammonium cation (Me2NH2 +), an hydrogenoxalate anion (HC2O4 −), and half a mol­ecule of oxalic acid (H2C2O4) situated about an inversion center. They are linked together through inter­molecular hydrogen bonds, forming a two-dimensional bilayer-like self-assembly.

crystal structureHydrogenInorganic chemistryOxalic acidSalt (chemistry)chemistry.chemical_elementCrystal structureHydrogenoxalateOxalateResearch Communicationschemistry.chemical_compoundGeneral Materials Sciencechemistry.chemical_classificationCrystallographyHydrogen bondGeneral ChemistryCondensed Matter Physicshydrogen bondingoxalic acid.CrystallographychemistryQD901-999organic saltdialkyammoniumMethanolhydrogenoxalateActa Crystallographica Section E: Crystallographic Communications
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Crystal structure and Hirshfeld surface analysis of a pyridiniminium bromide salt: 1-[2-(adamantan-1-yl)-2-oxoethyl]pyridin-4-iminium bromide

2018

The asymmetric unit of the title pyridiniminium halide salt comprise of one cation and one anion. In the crystal, mol­ecules are linked by N—H⋯Br and C—H⋯O hydrogen bonds, C—H⋯π inter­actions, and π–π inter­actions into layers. The inter­molecular inter­actions in the crystal structure are qu­anti­fied by Hirshfeld surface analysis.

crystal structureKetoneStackingCrystal structureDihedral angle010402 general chemistry01 natural sciencesResearch Communicationschemistry.chemical_compoundBromideMoietyHirshfeld surface analysisGeneral Materials Sciencepyridiniminium saltchemistry.chemical_classificationCrystallography010405 organic chemistryChemistryHydrogen bondIminiumGeneral ChemistryCondensed Matter Physicshydrogen bonding0104 chemical sciencesCrystallographyQD901-999Acta Crystallographica Section E: Crystallographic Communications
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Crystal structure and Hirshfeld surface analysis of (E)-3-[(4-fluorobenzylidene)amino]-5-phenylthiazolidin-2-iminium bromide

2019

TARAMAPUBMED TARAMASCOPUS TARAMAWOS In the cation of the title salt, C16H15FN3S+·Br−, the phenyl ring is disordered over two sets of sites with a refined occupancy ratio of 0.503 (4):0.497 (4). The mean plane of the thia­zolidine ring makes dihedral angles of 13.51 (14), 48.6 (3) and 76.5 (3)° with the fluoro­phenyl ring and the major- and minor-disorder components of the phenyl ring, respectively. The central thia­zolidine ring adopts an envelope conformation. In the crystal, centrosymmetrically related cations and anions are linked into dimeric units via N—H...Br hydrogen bonds, which are further connected by weak C—H...Br hydrogen bonds into chains parallel to [110]. Hirshfeld surface an…

crystal structureStackingCrystal structure010402 general chemistryRing (chemistry)01 natural sciencesCrystalHirshfeld surface analysis.chemistry.chemical_compoundBromideThia­zolidine ringcharge assisted hydrogen bondingHirshfeld surface analysisGeneral Materials ScienceBenzeneCrystallography010405 organic chemistryHydrogen bondIminiumdisorderGeneral ChemistryCondensed Matter::Mesoscopic Systems and Quantum Hall EffectCondensed Matter Physics0104 chemical sciencesCrystallographychemistryQD901-999thiazolidine ringActa Crystallographica Section E Crystallographic Communications
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