Search results for " diffraction"
showing 10 items of 896 documents
Single-zone-plate achromatic fresnel-transform setup: Pattern tunability
1997
Abstract White-light point-source illumination results in the chromatic blurring of the optical field diffracted by an aperture. In this paper, broadband dispersion compensation for a continuous set of Fresnel diffraction patterns associated with an arbitrary input transparency is carried out, in a sequential way, by means of a single on-axis blazed zone plate. The input is illuminated with a white-light converging spherical wavefront and the diffractive lens is inserted at the virtual source plane. We recognize that the position of the input along the optical axis permits to achieve a different achromatic Fresnel diffraction pattern with low residual chromatic aberrations. The theory deriv…
Totally incoherent optical processing operations with achromatic diffraction-based setups
2000
We report on a novel family of totally incoherent, chromatic-dispersion compensated hybrid (refractive-diffractive) lens setups for implementing, in the Fraunhofer or in the Fresnel diffraction region, different achromatic diffraction-based processing operations.
Three-dimensional behavior of apodized nontelecentric focusing systems.
2002
The scalar field in the focal volume of nontelecentric apodized focusing systems cannot be accurately described by the Debye integral representation. By use of the Fresnel–Kirchhoff diffraction formula it is found that, if the aperture stop is axially displaced, the focal-volume structure is tuned. We analyze the influence of the apodizing function and find that, whereas axially superresolving pupil filters are highly sensitive to the focal-volume reshaping effect, axially apodizing filters are more inclined to the focal-shift effect.
High-contrast white-light Lau fringes
2004
We present a new optical assembly with which to achieve Lau fringes with totally incoherent illumination. Gratinglike codification of the spatially incoherent source combined with an achromatic Fresnel diffraction setup allows us to achieve Lau fringe-pattern visibility of almost 100% with broadband light. The white-light character to our proposed setup is in stark contrast to previous monochromatic implementations. Potential implications of this fact are identified.
Undergraduate experiment with fractal diffraction gratings
2011
We present a simple diffraction experiment with fractal gratings based on the triadic Cantor set. Diffraction by fractals is proposed as a motivating strategy for students of optics in the potential applications of optical processing. Fraunhofer diffraction patterns are obtained using standard equipment present in most undergraduate physics laboratories and compared with those obtained with conventional periodic gratings. It is shown that fractal gratings produce self-similar diffraction patterns which can be evaluated analytically. Good agreement is obtained between experimental and numerical results. © 2011 IOP Publishing Ltd.
High-pressure theoretical and experimental study of HgWO4
2011
HgWO 4 at ambient pressure is characterized using a combination of ab initio calculations, X-ray diffraction and Raman scattering measurements. The effect of low pressure and temperature on the structural stability is analysed. Extending our ab initio study to the range of higher pressures, a sequence of stable phases up to 30GPa is proposed. © 2011 Taylor & Francis.
Synthesis of single crystalline sub-micron rutile TiO2 rods using hydrothermal treatment in acidic media
2014
Size engineered rutile sub-micron rods were obtained from nanostructured titania under acidic conditions. The synthesis was performed by hydrothermal treatment starting from TiO2-P25 and HCl. The synthesis proceeds in less than two hours and can be up-scaled to several grams in a one-pot reaction by increasing the reaction time. The product is single-phase, and the particles are single crystalline as confirmed by electron diffraction and powder X-ray diffraction analysis. The length of the particles can be varied over a wide range from 100 nm to 1.3 μm by changing the acid concentration. Particle growth is proposed to proceed by a dissolution-recrystallization process via soluble [TiCl6]2− …
The role of electron diffraction in zeolite structure determination
2006
Because electron diffraction can sample individual microcrystals, it is clear that this single crystal method can facilitate, in at least two ways, structure determination for inorganic materials, such as zeolites, that are preferentially microcrystalline. First, in a qualitative application, three-dimensional tilts of individual small crystals, to map the reciprocal lattice, greatly facilitates unit cell and space group determination when powder diffraction indexing programs fail. If incoherent multiple scattering leads to violation of systematic absences, these absences can be restored by collection of precession diffraction patterns based on the Vincent-Midgley method [1], as demonstrate…
Automated electron diffraction tomography - a new tool for nano crystal structure analysis
2011
Automated electron Diffraction Tomography (ADT) comprises an upcoming method for “ab intio” structure analysis of nano crystals. ADT allows fine sampling of the reciprocal space by sequential collection of electron diffraction patterns while tilting a nano crystal in fixed tilt steps around an arbitrary axis. Electron diffraction is collected in nano diffraction mode (NED) with a semi-parallel beam with a diameter down to 50 nm. For crystal tracking micro-probe STEM imaging is used. Full automation of the acquisition procedure allowed optimisation of the electron dose distribution and therefore analysis of highly beam sensitive samples. Cell parameters, space group and reflection intensitie…
Elucidating structural order and disorder phenomena in mullite-type Al4B2O9 by automated electron diffraction tomography
2017
The crystal structure and disorder phenomena of Al4B2O9, an aluminum borate from the mullite-type family, were studied using automated diffraction tomography (ADT), a recently established method for collection and analysis of electron diffraction data. Al4B2O9, prepared by sol-gel approach, crystallizes in the monoclinic space group C2/m. The ab initio structure determination based on three-dimensional electron diffraction data from single ordered crystals reveals that edge-connected AlO6 octahedra expanding along the b axis constitute the backbone. The ordered structure (A) was confirmed by TEM and HAADF-STEM images. Furthermore, disordered crystals with diffuse scattering along the b axis…