Search results for " diffraction"

White-light optical implementation of the fractional fourier transform with adjustable order control.

2000

An optical implementation of the fractional Fourier transform (FRT) with broadband illumination is proposed by use of a single imaging element, namely, a blazed diffractive lens. The setup displays an achromatized version of the FRT of order P of any two-dimensional input function. This fractional order can be tuned continuously by shifting of the input along the optical axis. Our compact and flexible configuration is tested with a chirplike input signal, and the good experimental results obtained support the theory.

Multi-illumination single-holographic-exposure lensless Fresnel (MISHELF) microscopy using 4 channels

2021

MISHELF microscopy is generalized by considering 4 illumination/detection channels while retaining single-shot working principle, twin image mitigation and noise averaging. Proof of principle validation is included considering a resolution test target.

Broadband space-variant Fresnel processor

2002

We present a radically new class of optical setup working with white-light illumination, namely, a chromatically compensated processor operating in the Fresnel domain. The optical configuration is a hybrid (diffractive-refractive) three-lens system that exhibits an intermediate achromatic Fresnel plane and an output image plane without chromatic distortion. As a first application of this optical arrangement we develop a parallel space-variant color pattern-recognition experiment with white light.

Specular reflection of spin-polarized electrons from the W(001) spin-filter crystal in a large range of scattering energies and angles

2015

Extending previous work on the imaging spin-filter technique based on electron diffraction from W(001) in the specular (00)-LEED (low-energy electron diffraction) spot, we studied the scattering-energy and angle-of-incidence landscape of spin sensitivity $S$ and reflectivity ${I/I}_{0}$. The setup includes a spin-polarized GaAs electron source and a rotatable delay-line detector for spatially resolving detection. We measured the intensity and spin asymmetry of the specularly reflected beam for energies between 14 and 37 eV and angles of incidence between ${30}^{\ensuremath{\circ}}$ and ${60}^{\ensuremath{\circ}}$. Resulting energy-angular landscapes show rather good agreement with theory [r…

Talbot interferometry: a new geometry

1993

Abstract With the Talbot effect, planes are found where the Fresnel diffraction pattern, of a Ronchi ruling, exhibits zero visibility. These planes are exploited to propose a novel geometry for Talbot interferometry, which has high sensitivity. Experimental verifications are included.

Brewster angle microscopy and X-ray GID studies of morphology and crystal structure in monolayers of N-tetradecyl-γ,δ-dihydroxypentanoic acid amide

1997

First-order phase transitions from the low-density fluidlike phase to the condensed phase of monolayers of N-tetradecyl-γ,δ-dihydroxypentanoic acid amides at the air−water interface have been studied by π−A isotherms, Brewster angle microscopy (BAM), and synchrotron X-ray grazing incidence diffraction (GID). The thermodynamic differences between enantiomeric and racemic monolayers are too small to be measured. However, chiral discrimination is observable in the macroscopic domain morphology by BAM. The domains of the condensed phase grow dendritically. The characteristic shapes of domains of the pure S and R enantiomers are mirror images of each other. The domains of the racemic mixture are…

Orientational Ordering ofN2OMolecules Adsorbed on Graphite (0001): A Novel Commensurate Pinwheel Structure

2000

The structure and orientational ordering of N2O molecules physisorbed on graphite (0001) is investigated applying x-ray, neutron, and low-energy electron diffraction techniques. Combining the results of the three techniques, we find that N2O forms a highly ordered, hexagonal, commensurate (sqrt[21]xsqrt[21])R10.89 degrees phase. The unit cell contains seven molecules which are arranged in a seven-sublattice pinwheel structure, unexpected for linear molecules on a hexagonal lattice. Potential energy calculations corroborate these results.

Synthesis and processing of nanocrystalline tungsten carbide: Towards cemented carbides with optimal mechanical properties

2011

Abstract Nanocrystalline tungsten carbide has been obtained by reduction/carburization at low temperature from precursors obtained by freeze-drying of aqueous solutions. Nanocrystalline WC powders with a adequate content of carbon were mixed with submicrometric Cobalt powder (12 wt.%), obtained by same synthesis method, and sintered in vacuum furnace. The cemented carbides fabricated from experimental powders were compared with both commercial ultrafine and nanocrystalline WC-12Co mixtures consolidated by the same route. The synthesised powders were characterized by X-ray powder diffraction, elemental analysis and scanning and high resolution transmission electron microscopy. On the other h…

Single-Crystal-to-Single-Crystal Anion Exchange in a Gadolinium MOF: Incorporation of POMs and [AuCl4]−

2016

The encapsulation of functional molecules inside porous coordination polymers (also known as metal-organic frameworks, MOFs) has become of great interest in recent years at the field of multifunctional materials. In this article, we present a study of the effects of size and charge in the anion exchange process of a Gd based MOF, involving molecular species like polyoxometalates (POMs), and [AuCl4]−. This post-synthetic modification has been characterized by IR, EDAX, and single crystal diffraction, which have provided unequivocal evidence of the location of the anion molecules in the framework.

Oxidative Addition of Halogens on Open Metal Sites in a Microporous Spin-Crossover Coordination Polymer

2009