Search results for "56"

showing 10 items of 1818 documents

CCDC 1826426: Experimental Crystal Structure Determination

2018

Related Article: Jie‐Shun Cui, Qian‐Kai Ba, Hua Ke, Arto Valkonen, Kari Rissanen, Wei Jiang|2018|Angew.Chem.,Int.Ed.|57|7809|doi:10.1002/anie.201803349

Space GroupCrystallography[2]-(N1-((35-di-t-butylphenyl)methyl)-N6-((4-(1-((35-di-t-butylphenyl)methyl)-1H-123-triazol-4-yl)phenyl)methyl)-N1N1N6N6-tetramethylhexane-16-diaminium)-(10163642-tetrabutoxy-28505456-tetraoxa-1339-diazoniatridecacyclo[43.7.1.1351.12327.12529.027.0611.01520.01924.03237.03355.04146.04953]hexapentaconta-246810151719212329(55)30323436414345(53)4648-icosaene)-rotaxane trifluoroacetate tris(hexafluorophosphate) acetone methanol dichloromethane solvate monohydrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1541408: Experimental Crystal Structure Determination

2017

Related Article: Gaël De Leener, Diana Over, Coryse Smet, Damien Cornut, Ana Gabriela Porras-Gutierrez, Isidoro López, Bénédicte Douziech, Nicolas Le Poul, Filip Topić, Kari Rissanen, Yves Le Mest, Ivan Jabin, and Olivia Reinaud|2017|Inorg.Chem.|56|10971|doi:10.1021/acs.inorgchem.7b01225

Space GroupCrystallography[3915414765-hexa-t-butyl-616970-trimethoxy-193752-trioxa-22252831345558-heptaazanonacyclo[26.22.10.71739.1711.14549.16367.0551.01318.03843]heptaconta-1(51)247(69)81013151738404245(61)464863(70)6466-octadecaene-233356-trione]-zinc(ii) bis(trifluoromethanesulfonate) diethyl ether unknown solvate monohydrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1575262: Experimental Crystal Structure Determination

2018

Related Article: Yan-Long Ma, Hua Ke, Arto Valkonen, Kari Rissanen, Wei Jiang|2018|Angew.Chem.,Int.Ed.|57|709|doi:10.1002/anie.201711077

Space GroupCrystallography[3]-(11'-(decane-110-diyl)bis(14-diazabicyclo[2.2.2]octan-1-ium))-bis(10163642-tetrabutoxy-132839505456-hexaoxatridecacyclo[43.7.1.1351.12327.12529.027.0611.01520.01924.03237.03355.04146.04953]hexapentaconta-246810151719212329(55)30323436414345(53)4648-icosaene)-rotaxane bis(hexafluorophosphate) 12-dichloroethane acetonitrile solvateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1555957: Experimental Crystal Structure Determination

2017

Related Article: Disha Mungalpara, Arto Valkonen, Kari Rissanen, Stefan Kubik|2017|Chemical Science|8|6005|doi:10.1039/C7SC02700A

Space GroupCrystallographybis(tetra-n-butylammonium) dihydrogen diphosphate 6183042-tetramethyl-345815161720272829323940414449515355-icosa-azanonacyclo[43.3.1.125.1913.11417.12125.12629.13337.13841]hexapentaconta-1(49)2(56)39(55)101214(54)1521(53)222426(52)2733(51)343638(50)394547-icosaene-7193143-tetrone dimethyl sulfoxide unknown solvate hydrateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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4,5,6,7-Tetrahydro-isoxazolo-[4,5-c]-pyridines as a new class of cytotoxic Hsp90 inhibitors.

2014

Hsp90 is considered an interesting therapeutic target for anticancer drug development. Here we describe a new class of 4,5,6,7-tetrahydro-isoxazolo-[4,5-c]-pyridine compounds. A small library of derivatives has been synthesized and investigated. Some reported compounds show interesting properties combining both notable binding to Hsp90 and potent cell growth inhibitory activity. N-5 substitution with a 2,4 resorcinol carboxamide appears crucial for activity. Moreover, a derivative bearing a hydroxamic acid residue bound to C-3 amide portion was found to inhibit both Hsp90 and HDAC6.

Spectrometry Mass Electrospray IonizationMagnetic Resonance Spectroscopymedicine.drug_classStereochemistryPyridinesCarboxamideApoptosisResorcinolAnti-cancer drugschemistry.chemical_compoundResidue (chemistry)AmideDrug DiscoveryHeat shock protein 90 Anti-cancer drugs 4567-Tetrahydro-isoxazolo-[45-c]- pyridinesmedicineCytotoxic T cellHumansHeat shock protein 90HSP90 Heat-Shock ProteinsPharmacologyHydroxamic acidChemistryCell growthOrganic ChemistryGeneral MedicineNuclear magnetic resonance spectroscopy4 5 6 7-Tetrahydro-isoxazolo-[4 5-c]-pyridinesFlow CytometrySettore CHIM/08 - Chimica Farmaceuticahsp90Settore BIO/14 - Farmacologia4 5 6 7-Tetrahydro-isoxazolo-[4 5-c]-pyridines; Anti-cancer drugs; Heat shock protein 90;K562 CellsCell DivisionEuropean journal of medicinal chemistry
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Ziemie Prus w trakcie polskiej wojny sukcesyjnej i wojny siedmioletniej

2021

W trakcie licznych konfliktów zbrojnych rozegranych w osiemnastowiecznej Europie Prusy Wschodnie tylko raz były teatrem działań wojennych: latem 1757 r. – zimą 1758 r. Dwukrotnie jednak działania zbrojne toczyły się nad jej granicami, a w latach 1734-1735 przez prowincje pruską przechodziły transporty i oddziały walczących wojsk. Taka postawa nie przyniosła wówczas królowi pruskiemu żadnych korzyści, ale też uchroniła Prusy Wschodnie oraz jego mieszkańców przed ewentualnymi negatywnymi skutkami wojny na terytorium Rzeczpospolitej. Jednak ponad dwadzieścia lat później Prusy Wschodnie nie uniknęły już okrucieństw wojny. Król Fryderyk II atakiem w sierpniu 1756 r. na Saksonię chciał uprzedzić …

Stanisław LeszczyńskiRosjawojna siedmioletnia 1756-1763cesarzowa ElżbietaThe war of 1733-1735Frederick II HohenzollernWojna 1733-1735Frederick William HohenzollernRussiaPrussiaFryderyk II Hohenzollernseven-year war of 1756-1763cesarzowa AnnaEmpress ElisabethPrusyFryderyk Wilhelm HohenzollernEmpress Anna
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Phenotypic and genotypic study on antibiotic resistance and pathogenic factors of Staphylococcus aureus isolates from small ruminant mastitis milk in…

2021

Staphyloccoccus aureus is the major cause of mastitis in small ruminants in the Mediterranean farms causing severe losses to dairy industry. Antibiotic treatment has been the most common approach to control these infections. Aim of this study was to investigate antimicrobial resistance (AMR), virulence factors and biofilm-related genes of 84 Sicilian strains of S. aureus isolated from sheep and goats milk during two different periods δT1 (2006-2009) and δT2 (2013-2015). Kirby Bauer method and Polymerase Chain Reaction (PCR) were utilized to monitor AMR and related genes (mecA, tetK, tetM, ermA, ermC). Moreover, toxin genes (tsst-1, sea-see, seg-sej, and sep) and biofilm genes (bap, ica, sas…

Staphylococcus aureusStaphylococcus aureus; Antimicrobial resistance; Virulence factors BiofilmVirulence factorsTetracyclineSulfamethoxazoleSCCmecBiofilmBiologyTP368-456medicine.disease_causemedicine.diseaseAntimicrobial resistanceFood processing and manufactureArticleMicrobiologyMastitisMultiple drug resistanceAntibiotic resistanceStaphylococcus aureusmedicineStaphylococcus aureuVancomycinFood Sciencemedicine.drugItalian Journal of Food Safety
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A subunit of eukaryotic translation initiation factor 2α-phosphatase (CreP/PPP1R15B) regulates membrane traffic.

2012

The constitutive reverter of eIF2α phosphorylation (CReP)/PPP1r15B targets the catalytic subunit of protein phosphatase 1 (PP1c) to phosphorylated eIF2α (p-eIF2α) to promote its dephosphorylation and translation initiation. Here, we report a novel role and mode of action of CReP. We found that CReP regulates uptake of the pore-forming Staphylococcus aureus α-toxin by epithelial cells. This function was independent of PP1c and translation, although p-eIF2α was involved. The latter accumulated at sites of toxin attack and appeared conjointly with α-toxin in early endosomes. CReP localized to membranes, interacted with phosphomimetic eIF2α, and, upon overexpression, induced and decorated a pop…

Staphylococcus aureusanimal structuresEndosomePopulationPhosphataseBacterial ToxinsEukaryotic Initiation Factor-2EndosomesBiologyBiochemistryExocytosisProtein Structure SecondaryEukaryotic translationProtein Phosphatase 1Initiation factorAnimalsHumansPhosphorylationeducationPeptide Chain Initiation TranslationalMolecular Biologyeducation.field_of_studyCell MembraneTranslation (biology)Epithelial CellsCell BiologyCell biologyProtein Structure TertiaryProtein TransportPhosphorylationRabbitsK562 CellsThe Journal of biological chemistry
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Antiproliferative agents that interfere with the cell cycle at the G(1)-->S transition: further development and characterization of a small library o…

2008

In this continuation of our research on derivatives containing the stilbene privileged structure or that are derived from it, we report the results of further studies carried out on the previously initiated collection of compounds. We used a parallel synthetic approach to rapidly obtain small sets of compounds and started the annotation of the library in progress by calculating some physicochemical properties to be eventually correlated with biological activities. A pharmacophore for the antiproliferative activity was also built to summarize the features of the library. We evaluated the antiproliferative and pro-apoptotic activities of all compounds as well as the cell-cycle effects of some…

StereochemistryCellular differentiationAntineoplastic AgentsApoptosisHL-60 CellsBiochemistryS PhaseSmall Molecule Librarieschemistry.chemical_compoundInhibitory Concentration 50Biological profileCell Line TumorDrug DiscoveryStilbenespharmacophoresHumansGeneral Pharmacology Toxicology and PharmaceuticsPhosphorylationPharmacologyChemistryOrganic ChemistryG1 PhaseRetinoblastomaSmall Molecule LibrariesG1/S transitionCell DifferentiationCell cycleFlow CytometryCombinatorial chemistryantitumor agentAntiproliferative AgentsMolecular MedicineTriolcell cyclePharmacophoreC-C couplingK562 Cells
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Steviol glycosides and bioactive compounds of a beverage with exotic fruits and Stevia rebaudiana Bert. as affected by thermal treatment

2020

The aim of this study was to investigate the effects of thermal processing on physicochemical properties, steviol glycosides, bioactive compounds, and antioxidant capacity degradation of a beverage based on exotic fruit juices, orange juice, açaí, and oat and sweetened with Stevia rebaudiana water extracts at different concentrations. The experimental design comprised a response surface methodology according to a central composite face-centered design. The variable ranges were 60–99°C, 0.25–15 min, 0–2.5% Stevia percentage. This design was used to determine the optimal thermal processing-Stevia concentration in order to obtain the best retention of bioactive compounds and physicochemical pr…

Steviollcsh:TX341-641Thermal treatmentphysicochemical properties01 natural scienceschemistry.chemical_compound0404 agricultural biotechnologyFood sciencethermal processingsteviol glycosideschemistry.chemical_classificationbioactive compoundslcsh:TP368-456stevia rebaudiana bertoni010401 analytical chemistryGlycoside04 agricultural and veterinary sciences040401 food science0104 chemical sciencesStevia rebaudianaAntioxidant capacitylcsh:Food processing and manufacturechemistrytotal antioxidant capacityexotic fruitslcsh:Nutrition. Foods and food supplyFood ScienceInternational Journal of Food Properties
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