Search results for "Automation"
showing 10 items of 1181 documents
Automated determination of reboxetine by high-performance liquid chromatography with column-switching and ultraviolet detection.
2000
A fully automated method including column-switching and isocratic high-performance liquid chromatography (HPLC) was developed for quantitative analysis of the new antidepressant reboxetine, a noradrenaline reuptake inhibitor. After serum injection into the HPLC system and on-line sample clean-up on a silica C8 (10x4.0 mm I.D.) clean-up column with an eluent consisting of 2.5% acetonitrile in deionized water, the chromatographic separation was performed on an analytical column (Lichrospher CN; 250x4.6 mm I.D.) with an eluent of acetonitrile-aqueous potassium phosphate buffer (0.008 M, pH 6.4) (50:50). The UV detector was set at 273 or 226 nm. The limit of quantification was about 15 ng/ml at…
Environmentally friendly analytical chemistry through automation: comparative study of strategies for carbaryl determination with p-aminophenol
1999
Abstract A flow system, based on multicommutation and binary sampling, has been developed for improving the automated spectrophotometric determination of carbaryl with p -aminophenol (PAP) in order to reduce the waste volume and to preserve the maximum analytical performance. The procedure, which was implemented employing a flow network obtained by nesting five, three-way solenoid valves controlled by means of a 386 microcomputer equipped with an electronic interface running software written in quick basic 4.5, provides a limit of detection of 26 μg l −1 , comparable to that obtained using a conventional flow injection (FIA) manifold and lower than that found by sequential injection analysi…
3D and multispectral imaging for subcutaneous veins detection.
2009
The first and perhaps most important phase of a surgical procedure is the insertion of an intravenous (IV) catheter. Currently, this is performed manually by trained personnel. In some visions of future operating rooms, however, this process is to be replaced by an automated system. Experiments to determine the best NIR wavelengths to optimize vein contrast for physiological differences such as skin tone and/or the presence of hair on the arm or wrist surface are presented. For illumination our system is composed of a mercury arc lamp coupled to a 10nm band-pass spectrometer. A structured lighting system is also coupled to our multispectral system in order to provide 3D information of the p…
Advances in automated diffraction tomography
2009
Crystal structure solution by means of electron diffraction or investigation of special structural features needs high quality data acquisition followed by data processing which delivers cell parameters, space group and in the end a 3D data set. The final step is the structure analysis itself including structure solution and subsequent refinement.
"Ab initio" structure solution from electron diffraction data obtained by a combination of automated diffraction tomography and precession technique
2009
Using a combination of our recently developed automated diffraction tomography (ADT) module with precession electron technique (PED), quasi-kinematical 3D diffraction data sets of an inorganic salt (BaSO(4)) were collected. The lattice cell parameters and their orientation within the data sets were found automatically. The extracted intensities were used for "ab initio" structure analysis by direct methods. The data set covered almost the complete set of possible symmetrically equivalent reflections for an orthorhombic structure. The structure solution in one step delivered all heavy (Ba, S) as well as light atoms (O). Results of the structure solution using direct methods, charge flipping …
Ab Initio Structure Determination of Vaterite by Automated Electron Diffraction
2012
tion that is fundamental for understanding material properties. Still, a number of compounds have eluded such kinds of analysis because they are nanocrystalline, highly disordered, with strong pseudosymmetries or available only in small amounts in polyphasic or polymorphic systems. These materials are crystallographically intractable with conventional Xray or synchrotron radiation diffraction techniques. Single nanoparticles can be visualized by high-resolution transmission electron microscopy (HR-TEM) up to sub�ngstrom resolution, [2] but obtaining 3D information is still a difficult task, especially for highly beam-sensitive materials and crystal structures with long cell parameters. Elec…
Marketing automation supporting sales
2016
The past couple of decades has been a time of major changes in marketing. Digitalization has become a permanent part of marketing and at the same time enabled efficient collection of data. Personalization and customization of content are playing a crucial role in marketing when new customers are acquired. This has also created a need for automation to facilitate the distribution of targeted content. As a result of successful marketing automation more information of the customers is gathered and at the same time, the work of sales force will be facilitated due to a larger amount of information. Marketing automation is used to support sales in modern companies, and specialized companies are a…
(p, 2)-Equations with a Crossing Nonlinearity and Concave Terms
2018
We consider a parametric Dirichlet problem driven by the sum of a p-Laplacian ($$p>2$$) and a Laplacian (a (p, 2)-equation). The reaction consists of an asymmetric $$(p-1)$$-linear term which is resonant as $$x \rightarrow - \infty $$, plus a concave term. However, in this case the concave term enters with a negative sign. Using variational tools together with suitable truncation techniques and Morse theory (critical groups), we show that when the parameter is small the problem has at least three nontrivial smooth solutions.
Information potential for some probability density functions
2021
Abstract This paper is related to the information theoretic learning methodology, whose goal is to quantify global scalar descriptors (e.g., entropy) of a given probability density function (PDF). In this context, the core concept is the information potential (IP) S [ s ] ( x ) : = ∫ R p s ( t , x ) d t , s > 0 of a PDF p(t, x) depending on a parameter x; it is naturally related to the Renyi and Tsallis entropies. We present several such PDF, viewed also as kernels of integral operators, for which a precise relation exists between S[2](x) and the variance Var[p(t, x)]. For these PDF we determine explicitly the IP and the Shannon entropy. As an application to Information Theoretic Learning w…
Adjacent vertices can be hard to find by quantum walks
2018
Quantum walks have been useful for designing quantum algorithms that outperform their classical versions for a variety of search problems. Most of the papers, however, consider a search space containing a single marked element. We show that if the search space contains more than one marked element, their placement may drastically affect the performance of the search. More specifically, we study search by quantum walks on general graphs and show a wide class of configurations of marked vertices, for which search by quantum walk needs Ω(N) steps, that is, it has no speed-up over the classical exhaustive search. The demonstrated configurations occur for certain placements of two or more adjace…