Search results for "Azepine"

showing 10 items of 266 documents

Development and evaluation of occlusive systems employing polyvinyl alcohol for transdermal delivery of sumatriptan succinate

2010

The aim of the present study was to develop a sumatriptan succinate transdermal system for applying migraine treatments efficiently and easily. For this system polyvinyl alcohol was employed as a matrix and Azone((R)) was added as a permeability enhancer. The physical characteristics, mechanical properties, and in vivo bioadhesion of the systems were evaluated, as was in vitro permeation across porcine skin. A uniform distribution of the drug in the matrix was observed, and moisture uptake values were constant. With regard to mechanical parameters, occlusive layer inclusion made the system more resistant, and no significant differences were detected with respect to other systems. Although A…

Materials scienceChemistry PharmaceuticalDrug CompoundingMigraine DisordersSkin AbsorptionPharmaceutical SciencePharmacologyAdministration CutaneousPolyvinyl alcoholPermeabilitychemistry.chemical_compoundDrug Delivery SystemsDrug StabilityIn vivoSumatriptan SuccinatemedicineTechnology PharmaceuticalVasoconstrictor AgentsDrug InteractionsAntihypertensive AgentsTransdermalDrug CarriersSumatriptanAzepinesGeneral MedicineHydrogen-Ion ConcentrationPermeationSerotonin Receptor AgonistsSumatriptanSolubilitychemistryPermeability (electromagnetism)Polyvinyl AlcoholPolyvinylsAzoneBiomedical engineeringmedicine.drugDrug Delivery
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ChemInform Abstract: Synthesis, Benzodiazepine Receptor Binding and Molecular Modelling of Isochromeno[4,3-c]pyrazol-5(1H)-one Derivatives.

2012

A series of isochromeno[4,3-c]pyrazol-5(1H)-one derivatives (III) is prepared and tested for their ability to displace specific [3H]flunitrazepam from bovine brain membranes.

MembraneBovine brainChemistryStereochemistrymedicineGeneral MedicineFlunitrazepamBenzodiazepine receptor bindingmedicine.drugChemInform
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Synthesis and antiproliferative activity of 3-(2-chloroethyl)-5-methyl-6-phenyl-8-(trifluoromethyl)-5,6-dihydropyrazolo[3,4-f][1,2,3,5]tetrazepin-4-(…

2015

Based on the encouraging results found for 3,5-dimethyl-6-phenyl-8-(trifluoromethyl)-5,6-dihydropyrazolo[3,4-f][1,2,3,5]tetrazepin-4-(3H)-one 7 previously tested by us, as well as the consideration that heterocycle fused tetrazepinones bearing the 2-chloroethyl substituent show a better cytotoxic profile than temozolomide and mitozolomide against human cancer cell lines which express the DNA repair protein O6-methylguanine-DNA methyltransferase (MGMT), in this paper we report the multistep synthesis and the biological study of 3-(2-cloroethyl)-5-methyl-6-phenyl-8-(trifluoromethyl)-5,6-dihydropyrazolo[3,4-f][1,2,3,5]tetrazepin-4-(3H)-one 10. Like compound 7, it was active on P-glycoprotein e…

MethyltransferaseStereochemistryHL60Antineoplastic AgentsApoptosisHL-60 CellsStructure-Activity Relationshipchemistry.chemical_compoundDrug DiscoveryHumansStructure–activity relationshipCell ProliferationPharmacologyTrifluoromethylDose-Response Relationship DrugMolecular StructureChemistryCell growthCell CycleOrganic ChemistryAzepinesGeneral MedicineCell cycleSettore CHIM/08 - Chimica Farmaceutica1235-Tetrazepinones pyrazolo[34-f][1235]-tetrazepinones drug resistance apoptosis antiproliferative activityCell cultureApoptosisPyrazolesDrug Screening Assays AntitumorK562 CellsEuropean Journal of Medicinal Chemistry
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Reduction of nevirapine-driven HIV mutations by carbamazepine is modulated by CYP3A activity

2014

Item does not contain fulltext OBJECTIVES: The reduction in mother-to-child transmission of HIV-1 by single-dose nevirapine given at birth onset is achieved at the expense of de novo HIV-1 resistance mutations. In the VITA1 study, single-dose carbamazepine accelerated nevirapine elimination, but the accompanying trend towards fewer de novo HIV-1 mutations was statistically non-significant. METHODS: We investigated if the effect of carbamazepine was confounded by the individual variability in nevirapine metabolism and transport. RESULTS: Nine of 34 (26%) single-dose nevirapine-treated women had one or more nevirapine-associated resistance mutations, compared with 3 of 34 (9%) in the single-d…

Microbiology (medical)NevirapineCYP3AAnti-HIV AgentsHuman immunodeficiency virus (HIV)Mutation MissenseEndogenyHIV InfectionsPharmacologyBiologymedicine.disease_causeChemopreventionPregnancyDrug Resistance ViralmedicineClinical endpointCytochrome P-450 CYP3AHumansPharmacology (medical)NevirapinePharmacologyMutationCYP3A4Cytochrome P-450 CYP3A InducersCarbamazepinelnfectious Diseases and Global Health Radboud Institute for Health Sciences [Radboudumc 4]Infectious DiseasesCarbamazepineTreatment OutcomeHIV-1Femalemedicine.drug
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5-(3,4-Dimethoxybenzyl)-7-isopropyl-1,3,5-triazepane-2,6-dione acetonitrile solvate refined using a multipolar atom model

2010

International audience; The crystal structure of the title compound, C16H23N3O4·CH3CN, was refined using a multipolar atom model transferred from an experimental electron-density database. The refinement showed some improvement in crystallographic statistical indices compared with the independent atom model. The triazepane ring adopts a twist-boat conformation. In the crystal structure, the mol­ecule forms inter­molecular contacts with 14 different neighbours. There are two N-H...O and one C-H...O inter­molecular hydrogen bond.

Models MolecularStereochemistryMolecular ConformationCrystal structure010402 general chemistryRing (chemistry)Crystallography X-Ray01 natural sciencesGeneral Biochemistry Genetics and Molecular Biologychemistry.chemical_compoundBenzyl Compounds[CHIM.CRIS]Chemical Sciences/CristallographyMoleculeAcetonitrileQuantitative Biology::Biomolecules010405 organic chemistryChemistryHydrogen bondIntermolecular forceGeneral MedicineAzepines0104 chemical sciencesCrystallographySolubilityDimerizationIsopropylAtom model
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Action of anticonvulsants on hippocampal slices in Mg-free medium

1989

The effects of six prototype anticonvulsant drugs were investigated on epileptiform field potential discharges evoked in hippocampal slices of rats by removing magnesium ions from the perfusion fluid in order to reveal a possible interaction with N-methyl-D-aspartate (NMDA) receptor activation. All drugs reduced the multiple discharges with the following order of potency: midazolam greater than carbamazepine = phenytoin = phenobarbital greater than ethosuximide = valproate. They had a stronger depressant effect on the later population spikes but none of them abolished the epileptiform discharge. These effects can be explained by known mechanisms of action of the anticonvulsants tested and l…

N-Methylaspartatemedicine.medical_treatmentPopulationPyramidal TractsIn Vitro TechniquesPharmacologyHippocampusReceptors N-Methyl-D-AspartatemedicineAnimalsMagnesiumeducationMagnesium ionPharmacologyAspartic Acideducation.field_of_studyEpilepsyDose-Response Relationship DrugChemistryElectroencephalographyRats Inbred StrainsGeneral MedicineCarbamazepineElectric StimulationRatsReceptors NeurotransmitterPerfusionEthosuximideAnticonvulsantnervous systemMechanism of actionNMDA receptorAnticonvulsantsPhenobarbitalmedicine.symptommedicine.drugNaunyn-Schmiedeberg's Archives of Pharmacology
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Synthesis of Azole-Heterocycles as Potential Antitumor and/or Antiviral Agents

2014

NNRTIantitumor agentoxazoleG-quadruplex ligandisoindolo[12-d][15]benzoxazepinetriazolesSettore CHIM/08 - Chimica Farmaceutica
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Uptake from water, biotransformation, and biliary excretion of pharmaceuticals by rainbow trout.

2011

An urgent need exists to assess the exposure of fish to pharmaceuticals. The aim of the present study was to assess the uptake and metabolism of waterborne pharmaceuticals in rainbow trout (Oncorhynchus mykiss). A further objective was to determine the possibility of monitoring exposure to low levels of pharmaceuticals by bile assays. Rainbow trout were exposed for 10 d under flow-through conditions to mixtures of five pharmaceuticals (diclofenac, naproxen, ibuprofen, bisoprolol, and carbamazepine) at high and low concentrations. The low concentration was used to mimic the conditions prevailing in the vicinity of the discharge points of wastewater treatment plants. The uptake and the biocon…

NaproxenDiclofenacHealth Toxicology and Mutagenesista1172BioconcentrationFresh WaterIbuprofenDiclofenacNaproxenBiotransformationBlood plasmamedicineEnvironmental ChemistryAnimalsBileBisoprololBiotransformationChromatographyChemistryMetabolismIbuprofenCarbamazepinePharmaceutical PreparationsEnvironmental chemistryOncorhynchus mykissRainbow troutWater Pollutants Chemicalmedicine.drugEnvironmental toxicology and chemistry
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Direct ELISA kits as a sensitive and selective screening method for abstinence control in urine.

2011

In 2009 cutoff values of assessment criteria to testify abstinence control in order to estimate driving ability were standardized in Germany. The cutoff values are lower than required in existing guidelines like SAMHSA and there is critical discussion about detection of low concentrations by using immunoassay, especially concerning amphetamines in urine (50 ng/ml). In this study Direct ELISA kits were tested for their applicability to identify the absence of amphetamines, cannabinoids, opiates, cocaine, methadone and benzodiazepines in urine. Results were confirmed by LC/MS or GC/MS analyses. Sensitivity, specificity, predictive values (positive as well as negative) and overall misclassific…

NarcoticsAnalyteAutomobile Drivingmedia_common.quotation_subjectPoison controlEnzyme-Linked Immunosorbent AssayUrineSensitivity and SpecificityGas Chromatography-Mass SpectrometryPathology and Forensic MedicineToxicologyBenzodiazepinesCocainePredictive Value of TestsmedicineCutoffHumansAmphetaminemedia_commonChromatographymedicine.diagnostic_testbusiness.industryAmphetaminesAbstinenceSubstance Abuse DetectionImmunoassayPredictive value of testsbusinessLawMethadonemedicine.drugForensic science international
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Unilateral multicystic dysplastic kidney in infants exposed to antiepileptic drugs during pregnancy

2007

Prenatal exposure to antiepileptic drugs (AEDs) increases the risk of major congenital malformations (MCM) in the fetus. AED-related abnormalities include heart and neural tube defects, cleft palate, and urogenital abnormalities. Among the various congenital anomalies of the kidney and urinary tract (CAKUT), multicystic dysplastic kidney (MCDK) disease is one of the most severe expressions. Although prenatal ultrasound (US) examination has increased the prenatal diagnosis of MCDK, the pathogenesis is still unclear. We report on four cases of MCDK in infants of epileptic women treated with AEDs during pregnancy. From October 2003 to June 2006, we observed four infants with unilateral MCDK bo…

Nephrologymedicine.medical_specialtyTime FactorsVoiding cystourethrogramUrinary systemMulticystic dysplastic kidneyPrenatal diagnosisUltrasonography PrenatalPregnancyInternal medicineProhibitinsmedicineHumansMulticystic Dysplastic KidneyMaternal-Fetal ExchangeFetusPregnancyEpilepsymedicine.diagnostic_testbusiness.industryObstetricsInfant Newbornmedicine.diseaseSurgeryMulticystic dysplastic kidney . Antiepileptic drugs . Major congenital anomalies . InfantCarbamazepineTreatment OutcomeNephrologyPhenobarbitalPrenatal Exposure Delayed EffectsPediatrics Perinatology and Child HealthGestationAnticonvulsantsFemalebusinessFollow-Up Studies
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