Search results for "Butanol"

showing 10 items of 71 documents

A Study of the Separation of 1-Dodecene and 1-Tetradecene Hydroformylation Products in Aqueous Medium

2009

Abstract Experimental results of the solubilization of olefins in hydroformylation model systems, comprising 1-dodecene and 1-tridecanal or 1-tetradecene and 1-pentadecanal, water, butanol, sodium dodecylsulfate (SDS), sodium dodecylbenzenesulfonate (SDBS), and/or tri(m-sulfofenyl)phosphine trisodium salt (TPPTS-Na) are presented. The selected systems were used for the hydroformylation of 1-dodecene and 1-tetradecene whereby high yields of aldehydes were obtained. After the reaction, the mixture spontaneously separated into an organic phase with the reaction products and an aqueous phase comprising the catalyst and excess phosphine ligand.

Process Chemistry and TechnologyGeneral Chemical EngineeringButanolSodium dodecylbenzenesulfonateAqueous two-phase systemFiltration and SeparationGeneral ChemistryCatalysischemistry.chemical_compoundchemistryOrganic chemistry1-DodeceneMicroemulsionPhosphineHydroformylationSeparation Science and Technology
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Vapor-liquid equilibria for the binary systems of methylcyclohexane with 1-propanol, 2-propanol, 1-butanol, and 2-butanol at 101.3 kPa

1997

Isobaric vapor−liquid equilibrium measurements at 101.3 kPa are reported for the binary systems methylcyclohexane + 1-propanol, + 2-propanol, + 1-butanol, and + 2-butanol. The systems show a strong positive deviation from ideality and present a minimum temperature azeotrope. The activity coefficients were found to be thermodynamically consistent by the methods of Van Ness−Byer−Gibbs and Wisniak. The date were correlated with five liquid-phase activity coefficient models (Margules, Van Laar, Wilson, NRTL, and UNIQUAC). According to the average deviations in temperature and in vapor composition the best model for the systems is NRTL.

PropanolActivity coefficientchemistry.chemical_compoundUNIQUACchemistryButanolAzeotropeGeneral Chemical EngineeringNon-random two-liquid modelThermodynamicsGeneral ChemistryMethylcyclohexane2-Butanol
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Evidence for the Existence of an Effective Interfacial Tension between Miscible Fluids: Isobutyric Acid-Water and 1-Butanol-Water in a Spinning-Drop …

2006

We report definitive evidence for an effective interfacial tension between two types of miscible fluids using spinning-drop tensiometry (SDT). Isobutyric acid (IBA) and water have an upper critical solution temperature (UCST) of 26.3 degrees C. We created a drop of the IBA-rich phase in the water-rich phase below the UCST and then increased the temperature above it. Long after the fluids have reached thermal equilibrium, the drop persists. By plotting the inverse of the drop radius cubed (r(-)(3)) vs the rotation rate squared (omega(2)), we confirmed that an interfacial tension exists and estimated its value. The transition between the miscible fluids remained sharp instead of becoming more…

SURFACE-TENSIONThermodynamicsGRADIENTSInstabilityIsobutyric acidSurface tensionchemistry.chemical_compoundNONEQUILIBRIUM FLUCTUATIONS1-ButanolIsobutyratesGRAVITYUpper critical solution temperatureElectrochemistrySurface TensionGeneral Materials ScienceSpectroscopyThermal equilibriumAqueous solutionDrop (liquid)ButanolDIFFUSION-COEFFICIENTWaterSurfaces and InterfacesCondensed Matter PhysicsKORTEWEG STRESSESLIGHT-SCATTERINGCAPILLARY TUBESButyrateschemistrySolubilityLIQUID-MIXTURESSYSTEM
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CCDC 966355: Experimental Crystal Structure Determination

2015

Related Article: Alexander Jeremies, Ulrike Lehmann, Sina Gruschinski, Frederik Schleife, Michel Meyer, Vitaly Matulis, Oleg A. Ivashkevich, Marcel Handke, Karolin Stein, Berthold Kersting|2015|Inorg.Chem.|54|3937|doi:10.1021/acs.inorgchem.5b00123

Space GroupCrystallography(mu-1531-di-t-butyl-723-dimethyl-3711192327-hexaazatricyclo[27.3.1.11317]tetratriaconta-1(33)13(34)14162931-hexaene-3334-dithiolato)-di-nickel diiodide t-butanol methanol solvateCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1483890: Experimental Crystal Structure Determination

2016

Related Article: Britta Glowacki, Michael Lutter, Dieter Schollmeyer, Wolf Hiller, and Klaus Jurkschat|2016|Inorg.Chem.|55|10218|doi:10.1021/acs.inorgchem.6b01429

Space GroupCrystallographyCrystal System(mu3-oxido)-(mu3-t-butanolato)-tris(mu2-bis(2-dimethyl-2-oxidopropyl)(1-dimethyl-2-oxidopropyl)amine)-tri-tin (mu3-oxido)-(mu3-bis(2-dimethyl-2-oxidopropyl)(1-dimethyl-2-oxidopropyl)amine)-bis(mu2-bis(2-dimethyl-2-oxidopropyl)(1-dimethyl-2-oxidopropyl)amine)-(t-butanolato)-tri-tin toluene solvateCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 192867: Experimental Crystal Structure Determination

2002

Related Article: S.Fustero, B.Pina, E.Salavert, A.Navarro, M.C.R.de Arellano, A.S.Fuentes|2002|J.Org.Chem.|67|4667|doi:10.1021/jo025621k

Space GroupCrystallographyCrystal System2-Methyl-3-(4-methoxyanilino)-444-trifluorobutanolCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 776225: Experimental Crystal Structure Determination

2011

Related Article: N.K.Beyeh, M.Cetina, M.Lofman, M.Luostarinen, A.Shivanyuk, K.Rissanen|2010|Supramol.Chem.|22|737|doi:10.1080/10610278.2010.506543

Space GroupCrystallographyCrystal System5111723-tetrakis(n-propylammoniomethyl)-46101216182224-octahydroxy-281420-tetrapropylcalix(4)arene tetrachloride butanol solvate hemihydrateCrystal StructureCell ParametersExperimental 3D Coordinates
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CCDC 1547599: Experimental Crystal Structure Determination

2017

Related Article: Agris Be¯rzinš, Aija Trimdale, Artis Kons, Dace Zvanina|2017|Cryst.Growth Des.|17|5712|doi:10.1021/acs.cgd.7b00657

Space GroupCrystallographyCrystal SystemCrystal Structure3alpha7alpha12alpha-trihydroxy-5beta-cholan-24-oic acid methyl ester t-butanol solvateCell ParametersExperimental 3D Coordinates
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CCDC 776228: Experimental Crystal Structure Determination

2011

Related Article: N.K.Beyeh, M.Cetina, M.Lofman, M.Luostarinen, A.Shivanyuk, K.Rissanen|2010|Supramol.Chem.|22|737|doi:10.1080/10610278.2010.506543

Space GroupCrystallographyCrystal SystemCrystal StructureCell Parameters5111723-tetrakis(cyclo-hexylammoniomethyl)-46101216182224-octahydroxy-281420-tetrapentylcalix(4)arene tetrachloride butanol chloroform solvateExperimental 3D Coordinates
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CCDC 829592: Experimental Crystal Structure Determination

2013

Related Article: N. Kodiah Beyeh, Mario Cetina,Kari Rissanen|2012|Cryst.Growth Des.|12|4919|doi:10.1021/cg3008409

Space GroupCrystallographyCrystal SystemCrystal StructureCell ParametersExperimental 3D Coordinates(281420-Tetraethyl-46101216182224-octahydroxy-5101520-tetrakis((N-propylammonio)methyl)calix(4)resorcinarene) tetrapicrate butanol chloroform solvate hemihydrate
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